2,5-dimethyl-4-{[4-(5-methylpyrimidin-2-yl)-1,3-thiazol-2-yl]methyl}aniline

Base Information

Chemical Name:2,5-dimethyl-4-{[4-(5-methylpyrimidin-2-yl)-1,3-thiazol-2-yl]methyl}aniline
CAS No.:1421922-79-3
Molecular Formula:C₁₇H₁₈N₄S
Molecular Weight:310.423
Hs Code.:

Synonyms:2,5-dimethyl-4-{[4-(5-methylpyrimidin-2-yl)-1,3-thiazol-2-yl]methyl}aniline

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Chemical Property of 2,5-dimethyl-4-{[4-(5-methylpyrimidin-2-yl)-1,3-thiazol-2-yl]methyl}aniline

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Technology Process of 2,5-dimethyl-4-{[4-(5-methylpyrimidin-2-yl)-1,3-thiazol-2-yl]methyl}aniline

There total 5 articles about 2,5-dimethyl-4-{[4-(5-methylpyrimidin-2-yl)-1,3-thiazol-2-yl]methyl}aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1421922-78-2
2-[2-(2,5-dimethyl-4-nitrobenzyl)-1,3-thiazol-4-yl]-5-methylpyrimidine

: 1421922-79-3
2,5-dimethyl-4-{[4-(5-methylpyrimidin-2-yl)-1,3-thiazol-2-yl]methyl}aniline

Guidance literature:: With hydrogen; palladium(II) hydroxide; In ethanol; at 20 ℃; for 19h;

Reference yield:

: 16213-85-7
(2,5-dimethylphenyl)acetonitrile

: 1421922-79-3
2,5-dimethyl-4-{[4-(5-methylpyrimidin-2-yl)-1,3-thiazol-2-yl]methyl}aniline

Guidance literature:: Multi-step reaction with 4 steps

1: nitric acid / 0.5 h / Cooling with ice

2: hydrogenchloride; O,O-Diethyl hydrogen phosphorodithioate / ethyl acetate / 24 h / 20 °C

3: isopropyl alcohol / 1 h / 80 °C

4: hydrogen; palladium(II) hydroxide / ethanol / 19 h / 20 °C

With hydrogenchloride; hydrogen; nitric acid; palladium(II) hydroxide; O,O-Diethyl hydrogen phosphorodithioate; In ethanol; ethyl acetate; isopropyl alcohol;

Reference yield:

: 1421922-03-3
(2,5-dimethyl-4-nitrophenyl)acetonitrile

: 1421922-79-3
2,5-dimethyl-4-{[4-(5-methylpyrimidin-2-yl)-1,3-thiazol-2-yl]methyl}aniline

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride; O,O-Diethyl hydrogen phosphorodithioate / ethyl acetate / 24 h / 20 °C

2: isopropyl alcohol / 1 h / 80 °C

3: hydrogen; palladium(II) hydroxide / ethanol / 19 h / 20 °C

With hydrogenchloride; hydrogen; palladium(II) hydroxide; O,O-Diethyl hydrogen phosphorodithioate; In ethanol; ethyl acetate; isopropyl alcohol;