Technology Process of C41H55N5O6
There total 3 articles about C41H55N5O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
hept-6-ynoic acid;
With
benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
at 20 ℃;
for 0.25h;
C34H47N5O5;
In
dichloromethane;
at 20 ℃;
DOI:10.1016/j.bmc.2012.09.020
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: trimethylphosphane / dichloromethane / 2 h / 20 °C / Inert atmosphere
2.1: sodium tris(acetoxy)borohydride / dichloromethane / 18 h / 20 °C
3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.25 h / 20 °C
3.2: 20 °C
With
sodium tris(acetoxy)borohydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trimethylphosphane;
In
dichloromethane;
DOI:10.1016/j.bmc.2012.09.020
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium tris(acetoxy)borohydride / dichloromethane / 18 h / 20 °C
2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.25 h / 20 °C
2.2: 20 °C
With
sodium tris(acetoxy)borohydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
DOI:10.1016/j.bmc.2012.09.020
