(3R,3aR,4R,10cR)-tert-butyl 4-(4-chlorobenzoyl)-3-(4-chlorophenyl)-3-hydroxy-2-oxo-1,3,3a,4,5,10c-hexahydrocyclopenta[c]carbazole-6(2H)-carboxylate

Base Information

Chemical Name:(3R,3aR,4R,10cR)-tert-butyl 4-(4-chlorobenzoyl)-3-(4-chlorophenyl)-3-hydroxy-2-oxo-1,3,3a,4,5,10c-hexahydrocyclopenta[c]carbazole-6(2H)-carboxylate
CAS No.:1360110-87-7
Molecular Formula:C₃₃H₂₉Cl₂NO₅
Molecular Weight:590.503
Hs Code.:

(3R,3aR,4R,10cR)-tert-butyl 4-(4-chlorobenzoyl)-3-(4-chlorophenyl)-3-hydroxy-2-oxo-1,3,3a,4,5,10c-hexahydrocyclopenta[c]carbazole-6(2H)-carboxylate

Synonyms:(3R,3aR,4R,10cR)-tert-butyl 4-(4-chlorobenzoyl)-3-(4-chlorophenyl)-3-hydroxy-2-oxo-1,3,3a,4,5,10c-hexahydrocyclopenta[c]carbazole-6(2H)-carboxylate

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Chemical Property of (3R,3aR,4R,10cR)-tert-butyl 4-(4-chlorobenzoyl)-3-(4-chlorophenyl)-3-hydroxy-2-oxo-1,3,3a,4,5,10c-hexahydrocyclopenta[c]carbazole-6(2H)-carboxylate

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Technology Process of (3R,3aR,4R,10cR)-tert-butyl 4-(4-chlorobenzoyl)-3-(4-chlorophenyl)-3-hydroxy-2-oxo-1,3,3a,4,5,10c-hexahydrocyclopenta[c]carbazole-6(2H)-carboxylate

There total 4 articles about (3R,3aR,4R,10cR)-tert-butyl 4-(4-chlorobenzoyl)-3-(4-chlorophenyl)-3-hydroxy-2-oxo-1,3,3a,4,5,10c-hexahydrocyclopenta[c]carbazole-6(2H)-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₃H₂₉Cl₂NO₅

: C₃₃H₂₉Cl₂NO₅

: 1360110-87-7
(3R,3aR,4R,10cR)-tert-butyl 4-(4-chlorobenzoyl)-3-(4-chlorophenyl)-3-hydroxy-2-oxo-1,3,3a,4,5,10c-hexahydrocyclopenta[c]carbazole-6(2H)-carboxylate

Guidance literature:: With 2-pentafluorophenyl-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]triazol-2-ium tetrafluoroborate; sodium acetate; In toluene; at 50 ℃; for 40h; optical yield given as %de; enantioselective reaction;
DOI:10.1021/ol300192p

Reference yield:

: 5465-37-2,15331-50-7,27297-60-5
(E)-1,4-bis(4-chlorophenyl)but-2-ene-1,4-dione

: C₃₃H₂₉Cl₂NO₅

: 1360110-87-7
(3R,3aR,4R,10cR)-tert-butyl 4-(4-chlorobenzoyl)-3-(4-chlorophenyl)-3-hydroxy-2-oxo-1,3,3a,4,5,10c-hexahydrocyclopenta[c]carbazole-6(2H)-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: (R)-2-(diphenyl(trimethylsilyloxy)methyl)pyrrolidine; mesitylenecarboxylic acid / toluene / 48 h / 40 °C

2: 2-pentafluorophenyl-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]triazol-2-ium tetrafluoroborate; sodium acetate / toluene / 40 h / 50 °C

With 2-pentafluorophenyl-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]triazol-2-ium tetrafluoroborate; (R)-2-(diphenyl(trimethylsilyloxy)methyl)pyrrolidine; mesitylenecarboxylic acid; sodium acetate; In toluene;
DOI:10.1021/ol300192p

Reference yield:

: 1360110-51-5
tert-butyl 2-methyl-3-(3-oxoprop-1-enyl)-1H-indole-1-carboxylate

: C₃₃H₂₉Cl₂NO₅

: 1360110-87-7
(3R,3aR,4R,10cR)-tert-butyl 4-(4-chlorobenzoyl)-3-(4-chlorophenyl)-3-hydroxy-2-oxo-1,3,3a,4,5,10c-hexahydrocyclopenta[c]carbazole-6(2H)-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: (R)-2-(diphenyl(trimethylsilyloxy)methyl)pyrrolidine; mesitylenecarboxylic acid / toluene / 48 h / 40 °C

2: 2-pentafluorophenyl-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]triazol-2-ium tetrafluoroborate; sodium acetate / toluene / 40 h / 50 °C

With 2-pentafluorophenyl-6,7-dihydro-5H-pyrrolo[2,1-c][1,2,4]triazol-2-ium tetrafluoroborate; (R)-2-(diphenyl(trimethylsilyloxy)methyl)pyrrolidine; mesitylenecarboxylic acid; sodium acetate; In toluene;
DOI:10.1021/ol300192p