Technology Process of riccardiphenol B
There total 10 articles about riccardiphenol B which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride;
In
dimethyl sulfoxide;
at 110 ℃;
for 6h;
Inert atmosphere;
Sealed vial;
DOI:10.1021/ja110054q
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: tetrahydrofuran / 0.08 h / 22 °C / Inert atmosphere
1.2: 12 h / Inert atmosphere
2.1: sodium tetrahydroborate; water / tetrahydrofuran / 0 °C / Inert atmosphere
3.1: n-butyllithium / tetrahydrofuran / 0 - 22 °C / Inert atmosphere
3.2: -78 - 22 °C / Inert atmosphere
4.1: tetrahydrofuran / 0 - 22 °C / Inert atmosphere
5.1: pyridine; thionyl chloride / 1 h / 0 - 22 °C / Inert atmosphere
6.1: tetrabutyl ammonium fluoride / dimethyl sulfoxide / 6 h / 110 °C / Inert atmosphere; Sealed vial
With
pyridine; sodium tetrahydroborate; n-butyllithium; thionyl chloride; tetrabutyl ammonium fluoride; water;
In
tetrahydrofuran; dimethyl sulfoxide;
DOI:10.1021/ja110054q
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: n-butyllithium / tetrahydrofuran / 0 - 22 °C / Inert atmosphere
1.2: -78 - 22 °C / Inert atmosphere
2.1: tetrahydrofuran / 0 - 22 °C / Inert atmosphere
3.1: pyridine; thionyl chloride / 1 h / 0 - 22 °C / Inert atmosphere
4.1: tetrabutyl ammonium fluoride / dimethyl sulfoxide / 6 h / 110 °C / Inert atmosphere; Sealed vial
With
pyridine; n-butyllithium; thionyl chloride; tetrabutyl ammonium fluoride;
In
tetrahydrofuran; dimethyl sulfoxide;
DOI:10.1021/ja110054q
