C₉H₇Br₂F₃

Base Information

Chemical Name:C₉H₇Br₂F₃
CAS No.:175990-24-6
Molecular Formula:C₉H₇Br₂F₃
Molecular Weight:331.958
Hs Code.:

C<sub>9</sub>H<sub>7</sub>Br<sub>2</sub>F<sub>3</sub>

Synonyms:C₉H₇Br₂F₃

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Chemical Property of C₉H₇Br₂F₃

Chemical Property:

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Technology Process of C₉H₇Br₂F₃

There total 1 articles about C₉H₇Br₂F₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 261952-19-6
4-(bromomethyl)-1-methyl-2-(trifluoromethyl)benzene

: 175990-24-6
C₉H₇Br₂F₃

Guidance literature:: With sodium bromate; sodium hydrogensulfite; In water; ethyl acetate; for 77h; Inert atmosphere;
DOI:10.1016/j.bmc.2014.02.054

Reference yield: 51.0%

: 175990-24-6
C₉H₇Br₂F₃

: 122-52-1
triethyl phosphite

: 1601462-25-2
C₁₇H₂₇F₃O₆P₂

Guidance literature:: at 150 ℃; for 16h; Inert atmosphere;
DOI:10.1016/j.bmc.2014.02.054

Reference yield:

: 175990-24-6
C₉H₇Br₂F₃

: 170661-02-6
(E,E)-1-trifluoromethyl-2,5-bis(4-hydroxy)styrylbenzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: 16 h / 150 °C / Inert atmosphere

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0 °C / Inert atmosphere

2.2: 16 h / 20 °C / Inert atmosphere

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 16 h / 0 - 20 °C / Inert atmosphere

With tetrabutyl ammonium fluoride; sodium hydride; In tetrahydrofuran; mineral oil; 1.1: |Arbuzov Reaction / 2.2: |Horner-Wadsworth-Emmons Olefination;
DOI:10.1016/j.bmc.2014.02.054