methyl 3-methoxy-4-<3-<2-<4-<2-methoxy-5-(1,3-dioxan-2-yl)phenoxy>phenyl>ethenyl>phenoxy>benzoate

Base Information

Chemical Name:methyl 3-methoxy-4-<3-<2-<4-<2-methoxy-5-(1,3-dioxan-2-yl)phenoxy>phenyl>ethenyl>phenoxy>benzoate
CAS No.:101613-53-0
Molecular Formula:C₃₄H₃₂O₈
Molecular Weight:568.623
Hs Code.:

Synonyms:methyl 3-methoxy-4-<3-<2-<4-<2-methoxy-5-(1,3-dioxan-2-yl)phenoxy>phenyl>ethenyl>phenoxy>benzoate

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Chemical Property of methyl 3-methoxy-4-<3-<2-<4-<2-methoxy-5-(1,3-dioxan-2-yl)phenoxy>phenyl>ethenyl>phenoxy>benzoate

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Technology Process of methyl 3-methoxy-4-<3-<2-<4-<2-methoxy-5-(1,3-dioxan-2-yl)phenoxy>phenyl>ethenyl>phenoxy>benzoate

There total 19 articles about methyl 3-methoxy-4-<3-<2-<4-<2-methoxy-5-(1,3-dioxan-2-yl)phenoxy>phenyl>ethenyl>phenoxy>benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 101554-01-2
methyl 3-methoxy-4-(3-formylphenoxy)benzoate

: 101554-00-1
diethyl <4-<2-methoxy-5-(1,3-dioxan-2-yl)phenoxy>benzyl>phosphonate

: 101613-53-0
4-(3-{(E)-2-[4-(5-[1,3]Dioxan-2-yl-2-methoxy-phenoxy)-phenyl]-vinyl}-phenoxy)-3-methoxy-benzoic acid methyl ester

Guidance literature:: With potassium tert-butylate; In N,N-dimethyl-formamide;
DOI:10.1246/cl.1985.1587

Reference yield:

: 621-59-0
isovanillin

: 101613-53-0
4-(3-{(E)-2-[4-(5-[1,3]Dioxan-2-yl-2-methoxy-phenoxy)-phenyl]-vinyl}-phenoxy)-3-methoxy-benzoic acid methyl ester

Guidance literature:: Multi-step reaction with 7 steps

1: 79 percent / K₂CO₃-CuO / pyridine / Heating

2: p-TsOH

3: LiAlH₄

4: SOBr₂

6: p-TsOH

7: 84 percent / t-BuOk / dimethylformamide

With lithium aluminium tetrahydride; sulfurous dibromide; potassium tert-butylate; potassium carbonate; copper(II) oxide; toluene-4-sulfonic acid; In pyridine; N,N-dimethyl-formamide;
DOI:10.1246/cl.1985.1587

Reference yield:

: 619-42-1
4-methoxycarbonylphenyl bromide

: 101613-53-0
4-(3-{(E)-2-[4-(5-[1,3]Dioxan-2-yl-2-methoxy-phenoxy)-phenyl]-vinyl}-phenoxy)-3-methoxy-benzoic acid methyl ester

Guidance literature:: Multi-step reaction with 7 steps

1: 79 percent / K₂CO₃-CuO / pyridine / Heating

2: p-TsOH

3: LiAlH₄

4: SOBr₂

6: p-TsOH

7: 84 percent / t-BuOk / dimethylformamide

With lithium aluminium tetrahydride; sulfurous dibromide; potassium tert-butylate; potassium carbonate; copper(II) oxide; toluene-4-sulfonic acid; In pyridine; N,N-dimethyl-formamide;
DOI:10.1246/cl.1985.1587