4-(bis(1,3-dipropyl-2-thioxo-2,3-dihydro-1H-benzo[d]imidazol-5-yl)amino)benzaldehyde

Base Information

Chemical Name:4-(bis(1,3-dipropyl-2-thioxo-2,3-dihydro-1H-benzo[d]imidazol-5-yl)amino)benzaldehyde
CAS No.:1400395-10-9
Molecular Formula:C₃₃H₃₉N₅OS₂
Molecular Weight:585.838
Hs Code.:

Synonyms:4-(bis(1,3-dipropyl-2-thioxo-2,3-dihydro-1H-benzo[d]imidazol-5-yl)amino)benzaldehyde

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Chemical Property of 4-(bis(1,3-dipropyl-2-thioxo-2,3-dihydro-1H-benzo[d]imidazol-5-yl)amino)benzaldehyde

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Technology Process of 4-(bis(1,3-dipropyl-2-thioxo-2,3-dihydro-1H-benzo[d]imidazol-5-yl)amino)benzaldehyde

There total 6 articles about 4-(bis(1,3-dipropyl-2-thioxo-2,3-dihydro-1H-benzo[d]imidazol-5-yl)amino)benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 1400395-08-5
5,5’-(phenylazanediyl)bis(1,3-dipropyl-1H-benzo[d]imidazole-2(3H)-thione)

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 1400395-10-9
4-(bis(1,3-dipropyl-2-thioxo-2,3-dihydro-1H-benzo[d]imidazol-5-yl)amino)benzaldehyde

Guidance literature:: With trichlorophosphate; In 1,2-dichloro-ethane; at 0 - 85 ℃; for 6h;
DOI:10.1021/ol4001685

Reference yield:

: 615-16-7
1,3-dihydro-2H-benzimidazol-2-one

: 1400395-10-9
4-(bis(1,3-dipropyl-2-thioxo-2,3-dihydro-1H-benzo[d]imidazol-5-yl)amino)benzaldehyde

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydroxide; tetrabutylammomium bromide / water; toluene / 10 h / 60 °C

2: sulfuric acid; iodine; sodium periodate / water; acetic acid / 8 h / 40 °C

3: copper(l) iodide; [2,2]bipyridinyl; potassium tert-butylate / toluene / 14 h / 140 °C / Sealed tube

4: Lawessons reagent / toluene / 12 h / 110 °C

5: trichlorophosphate / 1,2-dichloro-ethane / 6 h / 0 - 85 °C

With Lawessons reagent; [2,2]bipyridinyl; sodium periodate; copper(l) iodide; sulfuric acid; potassium tert-butylate; tetrabutylammomium bromide; iodine; sodium hydroxide; trichlorophosphate; In water; acetic acid; 1,2-dichloro-ethane; toluene;
DOI:10.1021/ol4001685

Reference yield:

: 95-54-5
1,2-diamino-benzene

: 1400395-10-9
4-(bis(1,3-dipropyl-2-thioxo-2,3-dihydro-1H-benzo[d]imidazol-5-yl)amino)benzaldehyde

Guidance literature:: Multi-step reaction with 6 steps

1: ethylene glycol / 8 h / 20 - 150 °C

2: sodium hydroxide; tetrabutylammomium bromide / water; toluene / 10 h / 60 °C

3: sulfuric acid; iodine; sodium periodate / water; acetic acid / 8 h / 40 °C

4: copper(l) iodide; [2,2]bipyridinyl; potassium tert-butylate / toluene / 14 h / 140 °C / Sealed tube

5: Lawessons reagent / toluene / 12 h / 110 °C

6: trichlorophosphate / 1,2-dichloro-ethane / 6 h / 0 - 85 °C

With Lawessons reagent; [2,2]bipyridinyl; sodium periodate; copper(l) iodide; sulfuric acid; potassium tert-butylate; tetrabutylammomium bromide; iodine; sodium hydroxide; trichlorophosphate; In water; ethylene glycol; acetic acid; 1,2-dichloro-ethane; toluene;
DOI:10.1021/ol4001685