1-(p-chlorophenyl)-3-(2'-chlorophenyl)-5-(3-phenyl-4-oxo-(3H)-quinazolin-2-mercaptoacetyl)formazan

Base Information

Chemical Name:1-(p-chlorophenyl)-3-(2'-chlorophenyl)-5-(3-phenyl-4-oxo-(3H)-quinazolin-2-mercaptoacetyl)formazan
CAS No.:1313265-52-9
Molecular Formula:C₂₉H₂₀Cl₂N₆O₂S
Molecular Weight:587.489
Hs Code.:

Synonyms:1-(p-chlorophenyl)-3-(2'-chlorophenyl)-5-(3-phenyl-4-oxo-(3H)-quinazolin-2-mercaptoacetyl)formazan

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Chemical Property of 1-(p-chlorophenyl)-3-(2'-chlorophenyl)-5-(3-phenyl-4-oxo-(3H)-quinazolin-2-mercaptoacetyl)formazan

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Technology Process of 1-(p-chlorophenyl)-3-(2'-chlorophenyl)-5-(3-phenyl-4-oxo-(3H)-quinazolin-2-mercaptoacetyl)formazan

There total 4 articles about 1-(p-chlorophenyl)-3-(2'-chlorophenyl)-5-(3-phenyl-4-oxo-(3H)-quinazolin-2-mercaptoacetyl)formazan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 106-47-8
4-chloro-aniline

: 56671-14-8
2-mercapto-2-(methylamido-2'-chloro-N-benzylidene)-3-phenyl-4-oxo-(3H)-quinazoline

: 1313265-52-9
1-(p-chlorophenyl)-3-(2'-chlorophenyl)-5-(3-phenyl-4-oxo-(3H)-quinazolin-2-mercaptoacetyl)formazan

Guidance literature:: 4-chloro-aniline; With hydrogenchloride; sodium nitrite; In water; acetic acid; at 0 - 5 ℃;

2-mercapto-2-(methylamido-2'-chloro-N-benzylidene)-3-phenyl-4-oxo-(3H)-quinazoline; With pyridine; In water; acetic acid; at 20 ℃;

Reference yield:

: 18741-24-7
2-mercapto-3-phenyl-3H-quinazolin-4-one

: 1313265-52-9
1-(p-chlorophenyl)-3-(2'-chlorophenyl)-5-(3-phenyl-4-oxo-(3H)-quinazolin-2-mercaptoacetyl)formazan

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / acetone / Reflux

2.1: hydrazine hydrate / ethanol / Reflux

3.1: acetic acid / methanol / Reflux

4.1: hydrogenchloride; sodium nitrite / water; acetic acid / 0 - 5 °C

4.2: 20 °C

With hydrogenchloride; potassium carbonate; hydrazine hydrate; acetic acid; sodium nitrite; In methanol; ethanol; water; acetic acid; acetone;

Reference yield:

: 37029-30-4
N-(3,4-Dihydro-4-oxo-3-phenylquinazolin-2-ylmercaptoacetyl)hydrazine

: 1313265-52-9
1-(p-chlorophenyl)-3-(2'-chlorophenyl)-5-(3-phenyl-4-oxo-(3H)-quinazolin-2-mercaptoacetyl)formazan

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic acid / methanol / Reflux

2.1: hydrogenchloride; sodium nitrite / water; acetic acid / 0 - 5 °C

2.2: 20 °C

With hydrogenchloride; acetic acid; sodium nitrite; In methanol; water; acetic acid;