methyl 2-(benzamido)-2-(1-benzyl-1H-1,2,3-triazol-4-yl)-3-phenylpropanoate

Base Information

Chemical Name:methyl 2-(benzamido)-2-(1-benzyl-1H-1,2,3-triazol-4-yl)-3-phenylpropanoate
CAS No.:1565852-25-6
Molecular Formula:C₂₆H₂₄N₄O₃
Molecular Weight:440.502
Hs Code.:

Synonyms:methyl 2-(benzamido)-2-(1-benzyl-1H-1,2,3-triazol-4-yl)-3-phenylpropanoate

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Chemical Property of methyl 2-(benzamido)-2-(1-benzyl-1H-1,2,3-triazol-4-yl)-3-phenylpropanoate

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Technology Process of methyl 2-(benzamido)-2-(1-benzyl-1H-1,2,3-triazol-4-yl)-3-phenylpropanoate

There total 3 articles about methyl 2-(benzamido)-2-(1-benzyl-1H-1,2,3-triazol-4-yl)-3-phenylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1565852-23-4
methyl 2-(benzamido)-2-benzylbut-3-ynoate

: 622-79-7
benzyl azide

: 1565852-25-6
methyl 2-(benzamido)-2-(1-benzyl-1H-1,2,3-triazol-4-yl)-3-phenylpropanoate

Guidance literature:: With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In dichloromethane; water; Schlenk technique; Inert atmosphere;
DOI:10.1021/ol500053c

Reference yield:

: 2566-22-5,2901-76-0,37002-52-1
DL-N-benzoylphenylalanine

: 1565852-25-6
methyl 2-(benzamido)-2-(1-benzyl-1H-1,2,3-triazol-4-yl)-3-phenylpropanoate

Guidance literature:: Multi-step reaction with 4 steps

1: acetic anhydride / Schlenk technique; Inert atmosphere

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.5 h / 20 °C / Schlenk technique; Inert atmosphere

3: potassium fluoride / 0.5 h / 55 °C / Schlenk technique; Inert atmosphere

4: copper(ll) sulfate pentahydrate; sodium L-ascorbate / dichloromethane; water / Schlenk technique; Inert atmosphere

With potassium fluoride; copper(ll) sulfate pentahydrate; acetic anhydride; sodium L-ascorbate; N-ethyl-N,N-diisopropylamine; In dichloromethane; water;
DOI:10.1021/ol500053c

Reference yield:

: 5874-61-3,21453-79-2,51127-19-6,75658-67-2
4-benzyl-2-phenyl-2-oxazolin-5-one

: 1565852-25-6
methyl 2-(benzamido)-2-(1-benzyl-1H-1,2,3-triazol-4-yl)-3-phenylpropanoate

Guidance literature:: Multi-step reaction with 3 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.5 h / 20 °C / Schlenk technique; Inert atmosphere

2: potassium fluoride / 0.5 h / 55 °C / Schlenk technique; Inert atmosphere

3: copper(ll) sulfate pentahydrate; sodium L-ascorbate / dichloromethane; water / Schlenk technique; Inert atmosphere

With potassium fluoride; copper(ll) sulfate pentahydrate; sodium L-ascorbate; N-ethyl-N,N-diisopropylamine; In dichloromethane; water;
DOI:10.1021/ol500053c