O-1-methyl-2-propynyl phenylphenylphosphinate

Base Information

Chemical Name:O-1-methyl-2-propynyl phenylphenylphosphinate
CAS No.:23834-42-6
Molecular Formula:C₁₆H₁₅O₂P
Molecular Weight:270.268
Hs Code.:

Synonyms:O-1-methyl-2-propynyl phenylphenylphosphinate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of O-1-methyl-2-propynyl phenylphenylphosphinate

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Technology Process of O-1-methyl-2-propynyl phenylphenylphosphinate

There total 3 articles about O-1-methyl-2-propynyl phenylphenylphosphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 2028-63-9
but-3-yn-2-ol

: 1499-21-4
Diphenylphosphinic chloride

: 23834-42-6
O-1-methyl-2-propynyl phenylphenylphosphinate

Guidance literature:: With triethylamine; trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/acs.organomet.5b00753

Reference yield: 87.0%

: 1707-03-5
diphenyl-phosphinic acid

: 2028-63-9
but-3-yn-2-ol

: 23834-42-6
O-1-methyl-2-propynyl phenylphenylphosphinate

Guidance literature:: With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine; In 1,2-dichloro-ethane; at 20 ℃; for 12h; Schlenk technique; Inert atmosphere;