(2S,3R)-3-[2-allyloxy-5-((1S,2S)-2-allyloxycarbonyl-1-(tert-butyl-dimethylsilanyloxy)-2-{methyl-[2-(trimethylsilanyl)ethoxycarbonyl]amino}ethyl)-phenoxy]-3-methyl-2-(2,2,2-trichloro-ethoxycarbonylamino)-pentanoic acid

Base Information

Chemical Name:(2S,3R)-3-[2-allyloxy-5-((1S,2S)-2-allyloxycarbonyl-1-(tert-butyl-dimethylsilanyloxy)-2-{methyl-[2-(trimethylsilanyl)ethoxycarbonyl]amino}ethyl)-phenoxy]-3-methyl-2-(2,2,2-trichloro-ethoxycarbonylamino)-pentanoic acid
CAS No.:1001431-16-8
Molecular Formula:C₃₇H₅₉Cl₃N₂O₁₁Si₂
Molecular Weight:870.412
Hs Code.:

(2S,3R)-3-[2-allyloxy-5-((1S,2S)-2-allyloxycarbonyl-1-(tert-butyl-dimethylsilanyloxy)-2-{methyl-[2-(trimethylsilanyl)ethoxycarbonyl]amino}ethyl)-phenoxy]-3-methyl-2-(2,2,2-trichloro-ethoxycarbonylamino)-pentanoic acid

Synonyms:(2S,3R)-3-[2-allyloxy-5-((1S,2S)-2-allyloxycarbonyl-1-(tert-butyl-dimethylsilanyloxy)-2-{methyl-[2-(trimethylsilanyl)ethoxycarbonyl]amino}ethyl)-phenoxy]-3-methyl-2-(2,2,2-trichloro-ethoxycarbonylamino)-pentanoic acid

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Chemical Property of (2S,3R)-3-[2-allyloxy-5-((1S,2S)-2-allyloxycarbonyl-1-(tert-butyl-dimethylsilanyloxy)-2-{methyl-[2-(trimethylsilanyl)ethoxycarbonyl]amino}ethyl)-phenoxy]-3-methyl-2-(2,2,2-trichloro-ethoxycarbonylamino)-pentanoic acid

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Technology Process of (2S,3R)-3-[2-allyloxy-5-((1S,2S)-2-allyloxycarbonyl-1-(tert-butyl-dimethylsilanyloxy)-2-{methyl-[2-(trimethylsilanyl)ethoxycarbonyl]amino}ethyl)-phenoxy]-3-methyl-2-(2,2,2-trichloro-ethoxycarbonylamino)-pentanoic acid

There total 1 articles about (2S,3R)-3-[2-allyloxy-5-((1S,2S)-2-allyloxycarbonyl-1-(tert-butyl-dimethylsilanyloxy)-2-{methyl-[2-(trimethylsilanyl)ethoxycarbonyl]amino}ethyl)-phenoxy]-3-methyl-2-(2,2,2-trichloro-ethoxycarbonylamino)-pentanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1001431-35-1
(2S,3R)-3-[2-allyloxy-5-((1S,2S)-2-allyloxycarbonyl-1-(tert-butyl-dimethylsilanyloxy)-2-{methyl-[2-(trimethylsilanyl)ethoxycarbonyl]amino}ethyl)-phenoxy]-3-methyl-2-(2,2,2-trichloro-ethoxycarbonylamino)-pentanoic acid tert-butyl ester

: 1001431-16-8
(2S,3R)-3-[2-allyloxy-5-((1S,2S)-2-allyloxycarbonyl-1-(tert-butyl-dimethylsilanyloxy)-2-{methyl-[2-(trimethylsilanyl)ethoxycarbonyl]amino}ethyl)-phenoxy]-3-methyl-2-(2,2,2-trichloro-ethoxycarbonylamino)-pentanoic acid

Guidance literature:: With silica gel; In toluene; for 37h; Heating;
DOI:10.1002/anie.200702537

Reference yield:

: 1001431-17-9
(2R,3S)-2-{(E)-[((S)-2,5-dihydro-1H-pyrrole-2-carbonyl)-amino]-3-methyl-pent-2-enoylamino}-3-hydroxy-succinic acid dimethyl ester

: 1001431-16-8
(2S,3R)-3-[2-allyloxy-5-((1S,2S)-2-allyloxycarbonyl-1-(tert-butyl-dimethylsilanyloxy)-2-{methyl-[2-(trimethylsilanyl)ethoxycarbonyl]amino}ethyl)-phenoxy]-3-methyl-2-(2,2,2-trichloro-ethoxycarbonylamino)-pentanoic acid

: 1001431-29-3
C₅₄H₈₂Cl₃N₅O₁₇Si₂

Guidance literature:: With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In acetonitrile; at 20 ℃; for 23h;
DOI:10.1002/anie.200702537