3-O-(2-arachidonyl-3-stearoyl-sn-glycerol-1-benzylphospahte)-1-O-dibenzylphosphate-2,4,6-O-tri-para-methoxybenzyl-D-myo-inositol

Base Information

• Chemical Name: 3-O-(2-arachidonyl-3-stearoyl-sn-glycerol-1-benzylphospahte)-1-O-dibenzylphosphate-2,4,6-O-tri-para-methoxybenzyl-D-myo-inositol
• CAS No.: 796883-99-3
• Molecular Formula: C₉₂H₁₂₆O₁₉P₂
• Molecular Weight: 1597.95

Synonyms:3-O-(2-arachidonyl-3-stearoyl-sn-glycerol-1-benzylphospahte)-1-O-dibenzylphosphate-2,4,6-O-tri-para-methoxybenzyl-D-myo-inositol

Chemical Property of 3-O-(2-arachidonyl-3-stearoyl-sn-glycerol-1-benzylphospahte)-1-O-dibenzylphosphate-2,4,6-O-tri-para-methoxybenzyl-D-myo-inositol

Chemical Property:

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Technology Process of 3-O-(2-arachidonyl-3-stearoyl-sn-glycerol-1-benzylphospahte)-1-O-dibenzylphosphate-2,4,6-O-tri-para-methoxybenzyl-D-myo-inositol

There total 2 articles about 3-O-(2-arachidonyl-3-stearoyl-sn-glycerol-1-benzylphospahte)-1-O-dibenzylphosphate-2,4,6-O-tri-para-methoxybenzyl-D-myo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

1-O-dibenzylphosphate-2,4,6-O-tri-para-methoxybenzyl-D-myo-inositol (796883-97-1) + (5Z,8Z,11Z,14Z)-Icosa-5,8,11,14-tetraenoic acid (S)-2-(benzyloxy-diisopropylamino-phosphanyloxy)-1-octadecanoyloxymethyl-ethyl ester → C140H203O26P3 + 3-O-(2-arachidonyl-3-stearoyl-sn-glycerol-1-benzylphospahte)-1-O-dibenzylphosphate-2,4,6-O-tri-para-methoxybenzyl-D-myo-inositol (796883-99-3)

Guidance literature:

1-O-dibenzylphosphate-2,4,6-O-tri-para-methoxybenzyl-D-myo-inositol; (5Z,8Z,11Z,14Z)-Icosa-5,8,11,14-tetraenoic acid (S)-2-(benzyloxy-diisopropylamino-phosphanyloxy)-1-octadecanoyloxymethyl-ethyl ester; With 4,5-dicyano-1H-imidazole; In dichloromethane; toluene;

With dihydrogen peroxide; In dichloromethane; toluene;

DOI:10.1021/jo060702s

Reference yield:

(5Z,8Z,11Z,14Z)-Icosa-5,8,11,14-tetraenoic acid (S)-2-{benzyloxy-[(1R,2R,3S,4R,5S,6S)-3-(bis-benzyloxy-phosphoryloxy)-5-hydroxy-2,4,6-tris-(4-methoxy-benzyloxy)-cyclohexyloxy]-phosphanyloxy}-1-octadecanoyloxymethyl-ethyl ester → 3-O-(2-arachidonyl-3-stearoyl-sn-glycerol-1-benzylphospahte)-1-O-dibenzylphosphate-2,4,6-O-tri-para-methoxybenzyl-D-myo-inositol (796883-99-3)

Guidance literature:

With dihydrogen peroxide; In dichloromethane; toluene; at 0 ℃; for 1h;

DOI:10.1021/ja0466098

Reference yield: 61.0%

3-O-(2-arachidonyl-3-stearoyl-sn-glycerol-1-benzylphospahte)-1-O-dibenzylphosphate-2,4,6-O-tri-para-methoxybenzyl-D-myo-inositol (796883-99-3) → (5Z,8Z,11Z,14Z)-Icosa-5,8,11,14-tetraenoic acid (S)-2-[hydroxy-((1R,2S,3R,4R,5S,6S)-2,3,4,6-tetrahydroxy-5-phosphonooxy-cyclohexyloxy)-phosphoryloxy]-1-octadecanoyloxymethyl-ethyl ester; compound with ammonia

Guidance literature:

With ammonium hydroxide; trimethylsilyl bromide; In toluene; at 70 ℃;

DOI:10.1021/jo060702s

upstream raw materials:

1-O-dibenzylphosphate-2,4,6-O-tri-para-methoxybenzyl-D-myo-inositol

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