C₄₅H₇₁SO₈SiN₃

Base Information

• Chemical Name: C₄₅H₇₁SO₈SiN₃
• CAS No.: 1092583-00-0
• Molecular Formula: C₄₅H₇₁N₃O₈SSi
• Molecular Weight: 842.226
• Mol file: 1092583-00-0.mol

Synonyms:C₄₅H₇₁SO₈SiN₃

Chemical Property of C₄₅H₇₁SO₈SiN₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₅H₇₁SO₈SiN₃

There total 26 articles about C₄₅H₇₁SO₈SiN₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C12H20O4 → C45H71SO8SiN3 (1092583-00-0)

Guidance literature:

Multi-step reaction with 10 steps

1.1: 95 percent / H₂ / Pd/C / ethyl acetate / 760.05 Torr

2.1: 91 percent / Et₃SiH; BF₃*OEt₂ / CH₂Cl₂ / 0 °C

3.1: 91 percent / LiAlH₄ / diethyl ether / 0 °C

4.1: 94 percent / I₂; PPh₃; imidazole / acetonitrile; benzene / 20 - 60 °C

5.1: t-BuLi / tetrahydrofuran / -78 °C

5.2: 95 percent / -78 - 0 °C

6.1: 89 percent / O₂ / PdCl₂; CuCl / H₂O; dimethylformamide

7.1: 98 percent / NaN₃ / dimethylsulfoxide / 50 °C

8.1: 89 percent / LiHMDS; Et₃N / tetrahydrofuran / -78 °C

9.1: 93 percent / MgBr₂*OEt₂ / CH₂Cl₂ / 0 °C

10.1: (cyclohexyl)2BCl; iPr₂NEt / CH₂Cl₂ / -78 °C

10.2: -78 - 0 °C

10.3: H₂O₂ / methanol / 0 - 20 °C / pH 7

With 1H-imidazole; triethylsilane; lithium aluminium tetrahydride; sodium azide; boron trifluoride diethyl etherate; dicyclohexylboron chloride; hydrogen; iodine; tert.-butyl lithium; oxygen; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; magnesium bromide; lithium hexamethyldisilazane; palladium on activated charcoal; copper(l) chloride; palladium dichloride; In tetrahydrofuran; diethyl ether; dichloromethane; water; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide; acetonitrile; benzene; 6.1: Wacker oxidation / 9.1: Mukaiyama aldol addition;

DOI:10.1002/anie.200701520

Reference yield:

C12H22O4 → C45H71SO8SiN3 (1092583-00-0)

Guidance literature:

Multi-step reaction with 9 steps

1.1: 91 percent / Et₃SiH; BF₃*OEt₂ / CH₂Cl₂ / 0 °C

2.1: 91 percent / LiAlH₄ / diethyl ether / 0 °C

3.1: 94 percent / I₂; PPh₃; imidazole / acetonitrile; benzene / 20 - 60 °C

4.1: t-BuLi / tetrahydrofuran / -78 °C

4.2: 95 percent / -78 - 0 °C

5.1: 89 percent / O₂ / PdCl₂; CuCl / H₂O; dimethylformamide

6.1: 98 percent / NaN₃ / dimethylsulfoxide / 50 °C

7.1: 89 percent / LiHMDS; Et₃N / tetrahydrofuran / -78 °C

8.1: 93 percent / MgBr₂*OEt₂ / CH₂Cl₂ / 0 °C

9.1: (cyclohexyl)2BCl; iPr₂NEt / CH₂Cl₂ / -78 °C

9.2: -78 - 0 °C

9.3: H₂O₂ / methanol / 0 - 20 °C / pH 7

With 1H-imidazole; triethylsilane; lithium aluminium tetrahydride; sodium azide; boron trifluoride diethyl etherate; dicyclohexylboron chloride; iodine; tert.-butyl lithium; oxygen; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; magnesium bromide; lithium hexamethyldisilazane; copper(l) chloride; palladium dichloride; In tetrahydrofuran; diethyl ether; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile; benzene; 5.1: Wacker oxidation / 8.1: Mukaiyama aldol addition;

DOI:10.1002/anie.200701520

Reference yield:

C10H18O3 → C45H71SO8SiN3 (1092583-00-0)

Guidance literature:

Multi-step reaction with 8 steps

1.1: 91 percent / LiAlH₄ / diethyl ether / 0 °C

2.1: 94 percent / I₂; PPh₃; imidazole / acetonitrile; benzene / 20 - 60 °C

3.1: t-BuLi / tetrahydrofuran / -78 °C

3.2: 95 percent / -78 - 0 °C

4.1: 89 percent / O₂ / PdCl₂; CuCl / H₂O; dimethylformamide

5.1: 98 percent / NaN₃ / dimethylsulfoxide / 50 °C

6.1: 89 percent / LiHMDS; Et₃N / tetrahydrofuran / -78 °C

7.1: 93 percent / MgBr₂*OEt₂ / CH₂Cl₂ / 0 °C

8.1: (cyclohexyl)2BCl; iPr₂NEt / CH₂Cl₂ / -78 °C

8.2: -78 - 0 °C

8.3: H₂O₂ / methanol / 0 - 20 °C / pH 7

With 1H-imidazole; lithium aluminium tetrahydride; sodium azide; dicyclohexylboron chloride; iodine; tert.-butyl lithium; oxygen; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; magnesium bromide; lithium hexamethyldisilazane; copper(l) chloride; palladium dichloride; In tetrahydrofuran; diethyl ether; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile; benzene; 4.1: Wacker oxidation / 7.1: Mukaiyama aldol addition;

DOI:10.1002/anie.200701520