Technology Process of Cobalt telluride
There total 22 articles about Cobalt telluride which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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In
neat (no solvent, solid phase);
byproducts: P(C2H5)3; in a tube under vacuum, heated at 300°C for 45 min, cooled; collected, washed with pentane, dried, X-ray powder diffraction, DSC, elem. anal.;
- Guidance literature:
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With
hydrazine hydrate;
In
water;
byproducts: Na2SO4, N2, H2O; High Pressure; Na2TeO3 added to soln. of Co salt in deionized H2O in an autoclave, stirred for 10 min, N2H4*H2O added, autoclave filled with H2O up to 80%, sealed, heated at 140°C for 5 h, allowed to cool to room temp.; filtered, washed with deionized H2O and abs. EtOH, dried at 60°C;XRD;
DOI:10.1021/ic0262031
- Guidance literature:
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heating Co shavings with powdered Te;;