3-(4-Chloro-phenyl)-2-[(E)-hydroxyimino]-3-oxo-N-(1-phenyl-ethyl)-thiopropionimidic acid methyl ester

Base Information

• Chemical Name: 3-(4-Chloro-phenyl)-2-[(E)-hydroxyimino]-3-oxo-N-(1-phenyl-ethyl)-thiopropionimidic acid methyl ester
• CAS No.: 112380-88-8
• Molecular Formula: C₁₈H₁₇ClN₂O₂S
• Molecular Weight: 360.864

Synonyms:3-(4-Chloro-phenyl)-2-[(E)-hydroxyimino]-3-oxo-N-(1-phenyl-ethyl)-thiopropionimidic acid methyl ester

Chemical Property of 3-(4-Chloro-phenyl)-2-[(E)-hydroxyimino]-3-oxo-N-(1-phenyl-ethyl)-thiopropionimidic acid methyl ester

Chemical Property:

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Technology Process of 3-(4-Chloro-phenyl)-2-[(E)-hydroxyimino]-3-oxo-N-(1-phenyl-ethyl)-thiopropionimidic acid methyl ester

There total 1 articles about 3-(4-Chloro-phenyl)-2-[(E)-hydroxyimino]-3-oxo-N-(1-phenyl-ethyl)-thiopropionimidic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

(Z)-1-(4-Chloro-phenyl)-3-methylsulfanyl-3-(1-phenyl-ethylamino)-propenone (112380-99-1) → 3-(4-Chloro-phenyl)-2-[(E)-hydroxyimino]-3-oxo-N-(1-phenyl-ethyl)-thiopropionimidic acid methyl ester (112380-88-8)

Guidance literature:

With pyridine; nitrosylchloride; In diethyl ether; chloroform; for 0.25h; Ambient temperature;

DOI:10.1055/s-1987-27998

Reference yield: 58.0%

3-(4-Chloro-phenyl)-2-[(E)-hydroxyimino]-3-oxo-N-(1-phenyl-ethyl)-thiopropionimidic acid methyl ester (112380-88-8) → (4-Chloro-phenyl)-(2-methyl-5-methylsulfanyl-2-phenyl-2H-imidazol-4-yl)-methanone (112380-76-4)

Guidance literature:

In acetonitrile; at 200 ℃; for 1h;

DOI:10.1055/s-1987-27998

upstream raw materials:

(Z)-1-(4-Chloro-phenyl)-3-methylsulfanyl-3-(1-phenyl-ethylamino)-propenone

Downstream raw materials:

(4-Chloro-phenyl)-(2-methyl-5-methylsulfanyl-2-phenyl-2H-imidazol-4-yl)-methanone

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