2-(benzo[d][1,3]dioxol-5-yl)-5-(biphenyl-4-ylmethylthio)-1,3,4-oxadiazole

Base Information

Chemical Name:2-(benzo[d][1,3]dioxol-5-yl)-5-(biphenyl-4-ylmethylthio)-1,3,4-oxadiazole
CAS No.:876687-00-2
Molecular Formula:C₂₂H₁₆N₂O₃S
Molecular Weight:388.447
Hs Code.:

Synonyms:2-(benzo[d][1,3]dioxol-5-yl)-5-(biphenyl-4-ylmethylthio)-1,3,4-oxadiazole

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Chemical Property of 2-(benzo[d][1,3]dioxol-5-yl)-5-(biphenyl-4-ylmethylthio)-1,3,4-oxadiazole

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Technology Process of 2-(benzo[d][1,3]dioxol-5-yl)-5-(biphenyl-4-ylmethylthio)-1,3,4-oxadiazole

There total 6 articles about 2-(benzo[d][1,3]dioxol-5-yl)-5-(biphenyl-4-ylmethylthio)-1,3,4-oxadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 2567-29-5
p-phenylbenzyl bromide

: 63698-52-2
2-mercapto-5-(3,4-methylenedioxyphenyl)-1,3,4-oxadiazole

: 876687-00-2
2-(benzo[d][1,3]dioxol-5-yl)-5-(biphenyl-4-ylmethylthio)-1,3,4-oxadiazole

Guidance literature:: With sodium hydroxide; In N,N-dimethyl-formamide; at 20 ℃; for 5h; Inert atmosphere;
DOI:10.1021/jm300309a

Reference yield:

: 94-53-1
Piperonylic acid

: 876687-00-2
2-(benzo[d][1,3]dioxol-5-yl)-5-(biphenyl-4-ylmethylthio)-1,3,4-oxadiazole

Guidance literature:: Multi-step reaction with 4 steps

1: 13 h / 0 - 50 °C

2: hydrazine hydrate / ethanol / 48 h / Reflux

3: triethylamine / ethanol / Reflux; Inert atmosphere

4: sodium hydroxide / N,N-dimethyl-formamide / 5 h / 20 °C / Inert atmosphere

With hydrazine hydrate; triethylamine; sodium hydroxide; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm300309a

Reference yield:

: 644-08-6
4-Methylbiphenyl

: 876687-00-2
2-(benzo[d][1,3]dioxol-5-yl)-5-(biphenyl-4-ylmethylthio)-1,3,4-oxadiazole

Guidance literature:: Multi-step reaction with 2 steps

1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 40 h / 80 °C / Inert atmosphere

2: sodium hydroxide / N,N-dimethyl-formamide / 5 h / 20 °C / Inert atmosphere

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); sodium hydroxide; In tetrachloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm300309a