<1S,(S)R>-1-(2-furyl)-1-O-<2'-trimethylsilylethoxy)methyl>-2-p-tolylsulfinylethanol

Base Information

Chemical Name:<1S,(S)R>-1-(2-furyl)-1-O-<2'-trimethylsilylethoxy)methyl>-2-p-tolylsulfinylethanol
CAS No.:160053-87-2
Molecular Formula:C₁₉H₂₈O₄SSi
Molecular Weight:380.58
Hs Code.:

Synonyms:<1S,(S)R>-1-(2-furyl)-1-O-<2'-trimethylsilylethoxy)methyl>-2-p-tolylsulfinylethanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of <1S,(S)R>-1-(2-furyl)-1-O-<2'-trimethylsilylethoxy)methyl>-2-p-tolylsulfinylethanol

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Technology Process of <1S,(S)R>-1-(2-furyl)-1-O-<2'-trimethylsilylethoxy)methyl>-2-p-tolylsulfinylethanol

There total 4 articles about <1S,(S)R>-1-(2-furyl)-1-O-<2'-trimethylsilylethoxy)methyl>-2-p-tolylsulfinylethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 76513-69-4
(2-trimethylethylsilylethoxy)methyl chloride

: 160053-85-0
<1S,(S)R>-1-(2-furyl)-2-p-tolylsulfinylethanol

: 160053-87-2
<1S,(S)R>-1-(2-furyl)-1-O-<2'-trimethylsilylethoxy)methyl>-2-p-tolylsulfinylethanol

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 40 ℃; for 5h;
DOI:10.1016/0957-4166(94)80033-2

Reference yield:

: 1519-39-7
(R)-methyl p-tolyl sulfoxide

: 160053-87-2
<1S,(S)R>-1-(2-furyl)-1-O-<2'-trimethylsilylethoxy)methyl>-2-p-tolylsulfinylethanol

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) LDA / 1.) THF, hexane, -78 deg C, 30 min, 2.) THF, hexane, 10 min

2: 85 percent / DIBALH / tetrahydrofuran / 5 h / -78 °C

3: 95 percent / diisopropylethylamine / CH₂Cl₂ / 5 h / 40 °C

With diisobutylaluminium hydride; N-ethyl-N,N-diisopropylamine; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane;
DOI:10.1016/0957-4166(94)80033-2

Reference yield:

: 614-99-3
Ethyl 2-furoate

: 160053-87-2
<1S,(S)R>-1-(2-furyl)-1-O-<2'-trimethylsilylethoxy)methyl>-2-p-tolylsulfinylethanol

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) LDA / 1.) THF, hexane, -78 deg C, 30 min, 2.) THF, hexane, 10 min

2: 85 percent / DIBALH / tetrahydrofuran / 5 h / -78 °C

3: 95 percent / diisopropylethylamine / CH₂Cl₂ / 5 h / 40 °C

With diisobutylaluminium hydride; N-ethyl-N,N-diisopropylamine; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane;
DOI:10.1016/0957-4166(94)80033-2