(2-Thien-3-ylphenyl)carbamic Acid 1-[2-(2-Chloro₄-formyl-5-methoxy-phenylcarbamoyl)ethyl]piperidin4-yl Ester

Base Information

• Chemical Name: (2-Thien-3-ylphenyl)carbamic Acid 1-[2-(2-Chloro₄-formyl-5-methoxy-phenylcarbamoyl)ethyl]piperidin4-yl Ester
• CAS No.: 876143-64-5
• Molecular Formula: C₂₇H₂₈ClN₃O₅S
• Molecular Weight: 542.055

Synonyms:(2-Thien-3-ylphenyl)carbamic Acid 1-[2-(2-Chloro₄-formyl-5-methoxy-phenylcarbamoyl)ethyl]piperidin4-yl Ester

Chemical Property of (2-Thien-3-ylphenyl)carbamic Acid 1-[2-(2-Chloro₄-formyl-5-methoxy-phenylcarbamoyl)ethyl]piperidin4-yl Ester

Chemical Property:

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Technology Process of (2-Thien-3-ylphenyl)carbamic Acid 1-[2-(2-Chloro₄-formyl-5-methoxy-phenylcarbamoyl)ethyl]piperidin4-yl Ester

There total 1 articles about (2-Thien-3-ylphenyl)carbamic Acid 1-[2-(2-Chloro₄-formyl-5-methoxy-phenylcarbamoyl)ethyl]piperidin4-yl Ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2-Thien-3-ylphenyl)carbamic Acid 1-[2-(2-Chloro-4-hydroxymethyl-5-methoxy-phenylcarbamoyl)ethyl]piperidin-4-yl Ester (1057248-85-7) → (2-Thien-3-ylphenyl)carbamic Acid 1-[2-(2-Chloro4-formyl-5-methoxy-phenylcarbamoyl)ethyl]piperidin4-yl Ester (876143-64-5)

Guidance literature:

(2-Thien-3-ylphenyl)carbamic Acid 1-[2-(2-Chloro-4-hydroxymethyl-5-methoxy-phenylcarbamoyl)ethyl]piperidin-4-yl Ester; With dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 ℃; for 0.25h;

With sulfur trioxide pyridine complex; In dichloromethane; for 1h;

With water; In dichloromethane;

Reference yield:

(2R)-2-{[tert-butyl(dimethyl)silyl]oxy}-2-(8-hydroxy-2-oxo-1,2-dihydroquinolin-5-yl)ethanaminium acetate + (2-Thien-3-ylphenyl)carbamic Acid 1-[2-(2-Chloro4-formyl-5-methoxy-phenylcarbamoyl)ethyl]piperidin4-yl Ester (876143-64-5) → (2-Thien-3-ylphenyl)carbamic Acid 1-[2-(4-{[(R)-2-(tert-butyldimethylsilanyloxy)-2-(8-hydroxy-2-oxo-1,2-dihydroquinolin-5-yl)ethylamino]methyl}-2-chloro-5-methoxy-phenylcarbamoyl)ethyl]piperidin-4-yl Ester (876143-65-6)

Guidance literature:

(2R)-2-{[tert-butyl(dimethyl)silyl]oxy}-2-(8-hydroxy-2-oxo-1,2-dihydroquinolin-5-yl)ethanaminium acetate; (2-Thien-3-ylphenyl)carbamic Acid 1-[2-(2-Chloro₄-formyl-5-methoxy-phenylcarbamoyl)ethyl]piperidin4-yl Ester; In methanol; dichloromethane; at 20 ℃; for 0.5h;

With sodium tris(acetoxy)borohydride; In methanol; dichloromethane; at 20 ℃; for 12h;

With sodium tetrahydroborate; acetic acid; more than 3 stages;

upstream raw materials:

(2-Thien-3-ylphenyl)carbamic Acid 1-[2-(2-Chloro-4-hydroxymethyl-5-methoxy-phenylcarbamoyl)ethyl]piperidin-4-yl Ester

Downstream raw materials:

(2-Thien-3-ylphenyl)carbamic Acid 1-[2-(4-{[(R)-2-(tert-butyldimethylsilanyloxy)-2-(8-hydroxy-2-oxo-1,2-dihydroquinolin-5-yl)ethylamino]methyl}-2-chloro-5-methoxy-phenylcarbamoyl)ethyl]piperidin-4-yl Ester

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