n-pentenyl <2,3-di-O-benzoyl-6-O-(2-naphthylmethyl)-β-D-galactopyranosyl>-(1<*>4)-2,3,6-tri-O-benzoyl-β-D-glucopyranoside

Base Information

Chemical Name:n-pentenyl <2,3-di-O-benzoyl-6-O-(2-naphthylmethyl)-β-D-galactopyranosyl>-(1<*>4)-2,3,6-tri-O-benzoyl-β-D-glucopyranoside
CAS No.:161767-02-8
Molecular Formula:C₆₃H₅₈O₁₆
Molecular Weight:1071.14
Hs Code.:

Synonyms:n-pentenyl <2,3-di-O-benzoyl-6-O-(2-naphthylmethyl)-β-D-galactopyranosyl>-(1<*>4)-2,3,6-tri-O-benzoyl-β-D-glucopyranoside

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Chemical Property of n-pentenyl <2,3-di-O-benzoyl-6-O-(2-naphthylmethyl)-β-D-galactopyranosyl>-(1<*>4)-2,3,6-tri-O-benzoyl-β-D-glucopyranoside

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Technology Process of n-pentenyl <2,3-di-O-benzoyl-6-O-(2-naphthylmethyl)-β-D-galactopyranosyl>-(1<*>4)-2,3,6-tri-O-benzoyl-β-D-glucopyranoside

There total 4 articles about n-pentenyl <2,3-di-O-benzoyl-6-O-(2-naphthylmethyl)-β-D-galactopyranosyl>-(1<*>4)-2,3,6-tri-O-benzoyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 161767-01-7
C₆₃H₅₆O₁₆

: 161767-02-8
n-pentenyl <2,3-di-O-benzoyl-6-O-(2-naphthylmethyl)-β-D-galactopyranosyl>-(1<*>4)-2,3,6-tri-O-benzoyl-β-D-glucopyranoside

Guidance literature:: With aluminium trichloride; trimethylamine-borane; 4 A molecular sieve; In tetrahydrofuran; Ambient temperature;
DOI:10.1016/S0957-4166(00)80383-3

Reference yield:

: 153228-87-6
n-pentenyl (β-D-galactopyranosyl)-(1<*>4)-β-D-glucopyranoside

: 161767-02-8
n-pentenyl <2,3-di-O-benzoyl-6-O-(2-naphthylmethyl)-β-D-galactopyranosyl>-(1<*>4)-2,3,6-tri-O-benzoyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 10-camphorsulfonic acid / 2 h / 55 °C

2: pyridine / 3 h / 0 - 20 °C

3: 95 percent / borane-trimethylamine complex, aluminum chloride, molecular sieves 4A / tetrahydrofuran / Ambient temperature

With pyridine; aluminium trichloride; trimethylamine-borane; 4 A molecular sieve; (1S)-10-camphorsulfonic acid; In tetrahydrofuran;
DOI:10.1016/S0957-4166(00)80383-3

Reference yield:

: 161767-00-6
2-naphthaldehyde di(isobutyl) acetal

: 161767-02-8
n-pentenyl <2,3-di-O-benzoyl-6-O-(2-naphthylmethyl)-β-D-galactopyranosyl>-(1<*>4)-2,3,6-tri-O-benzoyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 10-camphorsulfonic acid / 2 h / 55 °C

2: pyridine / 3 h / 0 - 20 °C

3: 95 percent / borane-trimethylamine complex, aluminum chloride, molecular sieves 4A / tetrahydrofuran / Ambient temperature

With pyridine; aluminium trichloride; trimethylamine-borane; 4 A molecular sieve; (1S)-10-camphorsulfonic acid; In tetrahydrofuran;
DOI:10.1016/S0957-4166(00)80383-3