(E)-methyl 3-(4-(benzyloxy)-3-bromophenyl)-2-(hydroxyimino)-propanoate

Base Information

Chemical Name:(E)-methyl 3-(4-(benzyloxy)-3-bromophenyl)-2-(hydroxyimino)-propanoate
CAS No.:1395312-68-1
Molecular Formula:C₁₇H₁₆BrNO₄
Molecular Weight:378.222
Hs Code.:

Synonyms:(E)-methyl 3-(4-(benzyloxy)-3-bromophenyl)-2-(hydroxyimino)-propanoate

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Chemical Property of (E)-methyl 3-(4-(benzyloxy)-3-bromophenyl)-2-(hydroxyimino)-propanoate

Chemical Property:

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Technology Process of (E)-methyl 3-(4-(benzyloxy)-3-bromophenyl)-2-(hydroxyimino)-propanoate

There total 2 articles about (E)-methyl 3-(4-(benzyloxy)-3-bromophenyl)-2-(hydroxyimino)-propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₇H₁₅BrO₄

: 1395312-68-1
(E)-methyl 3-(4-(benzyloxy)-3-bromophenyl)-2-(hydroxyimino)-propanoate

Guidance literature:: With hydroxylamine hydrochloride; In methanol; chloroform; at 20 ℃; for 19h; Inert atmosphere;
DOI:10.1039/c2ob25909e

Reference yield:

: methyl 3-(4-(benzyloxy)-3-bromophenyl)-2-(tert-butyldimethylsilyloxy)acrylate

: 1395312-68-1
(E)-methyl 3-(4-(benzyloxy)-3-bromophenyl)-2-(hydroxyimino)-propanoate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine tris(hydrogen fluoride) / methanol; chloroform / 0.5 h / 20 °C / Inert atmosphere

2: hydroxylamine hydrochloride / methanol; chloroform / 19 h / 20 °C / Inert atmosphere

With hydroxylamine hydrochloride; triethylamine tris(hydrogen fluoride); In methanol; chloroform;
DOI:10.1039/c2ob25909e

Reference yield:

: 1395312-68-1
(E)-methyl 3-(4-(benzyloxy)-3-bromophenyl)-2-(hydroxyimino)-propanoate

: 1395313-44-6
(Z)-methyl 3-(3-bromo-4-hydroxyphenyl)-2-(hydroxyimino)-propanoate

: 83030-43-7
(E)-methyl 3-(3-bromo-4-hydroxyphenyl)-2-(hydroxyimino)-propanoate

Guidance literature:: With palladium on activated charcoal; hydrogen; acetic acid; In 1,4-dioxane; at 20 ℃; for 41h; under 760.051 Torr; optical yield given as %de;
DOI:10.1039/c2ob25909e