((Z)-4-(tert-butyldimethylsilyloxy)but-2-enyl)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetimidate

Base Information

Chemical Name:((Z)-4-(tert-butyldimethylsilyloxy)but-2-enyl)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetimidate
CAS No.:1032191-88-0
Molecular Formula:C₁₉H₂₈F₃NO₃Si
Molecular Weight:403.517
Hs Code.:

Synonyms:((Z)-4-(tert-butyldimethylsilyloxy)but-2-enyl)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetimidate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ((Z)-4-(tert-butyldimethylsilyloxy)but-2-enyl)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetimidate

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Technology Process of ((Z)-4-(tert-butyldimethylsilyloxy)but-2-enyl)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetimidate

There total 1 articles about ((Z)-4-(tert-butyldimethylsilyloxy)but-2-enyl)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 91202-69-6,134297-05-5,113123-37-8
(Z)-4-(tert-butyldimethylsilyloxy)but-2-en-1-ol

: 75999-66-5
N-(4-methoxyphenyl)trifluoroacetimidoyl chloride

: 1032191-88-0
((Z)-4-(tert-butyldimethylsilyloxy)but-2-enyl)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetimidate

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1002/chem.200701642

Reference yield: 96.0%

: 1032191-88-0
((Z)-4-(tert-butyldimethylsilyloxy)but-2-enyl)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetimidate

: 1032192-19-0
(R)-N-(1-(tert-butyldimethylsilyloxy)but-3-en-2-yl)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetamide

Guidance literature:: With bis(di-μ-chloro-μ-{[bis-η⁵-(4'R,5'R)-(S_p)-2-(2'-4',5'-dihydro-4',5'-diphenyl-1'-tosyl-imidazolyl)cyclopentadienyl] iron(II) 1-C,3'-N} dipalladium(II)); silver(I) 4-methylbenzenesulfonate; In chloroform; at 55 ℃; for 72h; optical yield given as %ee; Inert atmosphere; Darkness;
DOI:10.1002/chem.200701642

Reference yield: 91.0%

: 1032191-88-0
((Z)-4-(tert-butyldimethylsilyloxy)but-2-enyl)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetimidate

: 1032191-91-5
rac-N-(1-(tert-butyldimethylsilyloxy)but-3-en-2-yl)-2,2,2-trifluoro-N-(4-methoxyphenyl)acetamide

Guidance literature:: With N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; In 1,3,5-trimethyl-benzene; at 160 ℃; for 43h;
DOI:10.1002/chem.200701642