O-Benzyl-N-{5-[bis-(5-benzyloxyamino-pentyl)-amino]-pentyl}-hydroxylamine

Base Information

• Chemical Name: O-Benzyl-N-{5-[bis-(5-benzyloxyamino-pentyl)-amino]-pentyl}-hydroxylamine
• CAS No.: 161561-27-9
• Molecular Formula: C₃₆H₅₄N₄O₃
• Molecular Weight: 590.85

Synonyms:O-Benzyl-N-{5-[bis-(5-benzyloxyamino-pentyl)-amino]-pentyl}-hydroxylamine

Chemical Property of O-Benzyl-N-{5-[bis-(5-benzyloxyamino-pentyl)-amino]-pentyl}-hydroxylamine

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Technology Process of O-Benzyl-N-{5-[bis-(5-benzyloxyamino-pentyl)-amino]-pentyl}-hydroxylamine

There total 3 articles about O-Benzyl-N-{5-[bis-(5-benzyloxyamino-pentyl)-amino]-pentyl}-hydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

N-Benzyloxy-N-(5-{bis-[5-(acetyl-benzyloxy-amino)-pentyl]-amino}-pentyl)-acetamide (161561-26-8) → O-Benzyl-N-{5-[bis-(5-benzyloxyamino-pentyl)-amino]-pentyl}-hydroxylamine (161561-27-9)

Guidance literature:

With barium dihydroxide; In methanol; for 72h;

DOI:10.1016/S0040-4039(00)78569-8

Reference yield:

1-Amino-5-pentane (83966-23-8) → O-Benzyl-N-{5-[bis-(5-benzyloxyamino-pentyl)-amino]-pentyl}-hydroxylamine (161561-27-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 65 percent / K₂CO₃ / acetonitrile / 24 h / Heating

2: 70 percent / Ba(OH)2*8H₂O / methanol / 72 h

With barium dihydroxide; potassium carbonate; In methanol; acetonitrile;

DOI:10.1016/S0040-4039(00)78569-8

Reference yield:

5--1-pentyl bromide (94136-48-8) → O-Benzyl-N-{5-[bis-(5-benzyloxyamino-pentyl)-amino]-pentyl}-hydroxylamine (161561-27-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 65 percent / K₂CO₃ / acetonitrile / 24 h / Heating

2: 70 percent / Ba(OH)2*8H₂O / methanol / 72 h

With barium dihydroxide; potassium carbonate; In methanol; acetonitrile;

DOI:10.1016/S0040-4039(00)78569-8

upstream raw materials:

N-Benzyloxy-N-(5-{bis-[5-(acetyl-benzyloxy-amino)-pentyl]-amino}-pentyl)-acetamide

1-Amino-5-pentane

5--1-pentyl bromide

Downstream raw materials:

1,13-Bis-benzyloxy-7-{5-[benzyloxy-(6-chloro-hexanoyl)-amino]-pentyl}-14,26-dioxo-1,7,13,20-tetraaza-cyclohexacosane-20-carboxylic acid 2,2,2-trichloro-1,1-dimethyl-ethyl ester

C₅₈H₈₆Cl₃N₅O₉

1,13-Bis-benzyloxy-7-(5-benzyloxyamino-pentyl)-14,26-dioxo-1,7,13,20-tetraaza-cyclohexacosane-20-carboxylic acid 2,2,2-trichloro-1,1-dimethyl-ethyl ester

7,21,32-Tris-benzyloxy-1,7,14,21,32-pentaaza-bicyclo[12.12.12]octatriacontane-8,20,33-trione

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