[η5-carbomethoxycyclopentadienyl][η4-1,3-bis(gem-diphenyltrifluorocyclotriphosphazenyl)-2,4-diphenylcyclobutadiene]cobalt

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Chemical Name:[η5-carbomethoxycyclopentadienyl][η4-1,3-bis(gem-diphenyltrifluorocyclotriphosphazenyl)-2,4-diphenylcyclobutadiene]cobalt
CAS No.:1312365-11-9
Molecular Formula:C₄₇H₃₇CoF₆N₆O₂P₆
Molecular Weight:1076.68
Hs Code.:

Synonyms:[η5-carbomethoxycyclopentadienyl][η4-1,3-bis(gem-diphenyltrifluorocyclotriphosphazenyl)-2,4-diphenylcyclobutadiene]cobalt

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Chemical Property of [η5-carbomethoxycyclopentadienyl][η4-1,3-bis(gem-diphenyltrifluorocyclotriphosphazenyl)-2,4-diphenylcyclobutadiene]cobalt

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Technology Process of [η5-carbomethoxycyclopentadienyl][η4-1,3-bis(gem-diphenyltrifluorocyclotriphosphazenyl)-2,4-diphenylcyclobutadiene]cobalt

There total 1 articles about [η5-carbomethoxycyclopentadienyl][η4-1,3-bis(gem-diphenyltrifluorocyclotriphosphazenyl)-2,4-diphenylcyclobutadiene]cobalt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

: 26305-75-9
chlorotris(triphenylphosphine)cobalt(I)

: 1312365-10-8
(β-phenylethynyl)-gem-diphenyltrifluorocyclotriphosphazene

: sodium (methoxycarbonyl)cyclopentadienide

: 1312365-11-9
[η5-carbomethoxycyclopentadienyl][η4-1,3-bis(gem-diphenyltrifluorocyclotriphosphazenyl)-2,4-diphenylcyclobutadiene]cobalt

: [cobalt(η5-carbomethylcyclopentadienyl)C4(Ph)2(gem-diphenyltrifluoro cyclotriphosphazenyl)(PNP(F)2NP(Ph)2N)]

: [cobalt(η5-carbomethylcyclopentadienyl)(gem-diphenyltrifluoro cycltriphosphazenyl)2C4(phenyl)2]

: [cobalt(η5-carbomethylcyclopentadienyl)(gem-diphenyltrifluoro cycltriphosphazenyl)2C4(phenyl)2]

Guidance literature:: In tetrahydrofuran; toluene; byproducts: triphenylphoshine, triphenylphosphine oxide; Schlenk technique, under N2; soln. of (C6H5CC)P(F)NP(F)2NP(C6H5)2N (3.1 mmol) and CoCl(PPh3)3 (1.67 mmol) (toluene) added to soln. of Na(C5H4COOCH3) (1.67 mmol) (THF) at stirring, stirred at room temp. for 15 min, refluxed for 24 h; solvents removed under vac., residue chromd. (alumina, hexane, then ethylacetate/hexane eluent), crystd. at slow evapn. satd. solns. (ethyl acetate/hexane); elem. anal.;
DOI:10.1016/j.ica.2011.01.064