(2S,3R)-2-benzyloxycarbonylamino-3-(4-benzyloxyphenyl)-3-hydroxypropioic acid

Base Information

Chemical Name:(2S,3R)-2-benzyloxycarbonylamino-3-(4-benzyloxyphenyl)-3-hydroxypropioic acid
CAS No.:444154-77-2
Molecular Formula:C₂₄H₂₃NO₆
Molecular Weight:421.45
Hs Code.:

Synonyms:(2S,3R)-2-benzyloxycarbonylamino-3-(4-benzyloxyphenyl)-3-hydroxypropioic acid

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Chemical Property of (2S,3R)-2-benzyloxycarbonylamino-3-(4-benzyloxyphenyl)-3-hydroxypropioic acid

Chemical Property:

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Technology Process of (2S,3R)-2-benzyloxycarbonylamino-3-(4-benzyloxyphenyl)-3-hydroxypropioic acid

There total 1 articles about (2S,3R)-2-benzyloxycarbonylamino-3-(4-benzyloxyphenyl)-3-hydroxypropioic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 621-84-1
O-benzyl carbamate

: 104315-07-3
(E)-ethyl 3-(4-(benzyloxy)phenyl)acrylate

: 444154-77-2
(2S,3R)-2-benzyloxycarbonylamino-3-(4-benzyloxyphenyl)-3-hydroxypropioic acid

Guidance literature:: O-benzyl carbamate; (E)-ethyl 3-(4-(benzyloxy)phenyl)acrylate; With sodium hydroxide; hydroquinidine anthraquinone-1,4-diyl diether; tert-butylhypochlorite; K2; In propan-1-ol; water; at 20 ℃; for 2h;

With lithium hydroxide; In tetrahydrofuran; water; at 0 ℃; for 1h; Further stages.;
DOI:10.1021/jo0256078

Reference yield: 64.0%

: β-alanyl-β-alanine methyl ester hydrochloride

: 444154-77-2
(2S,3R)-2-benzyloxycarbonylamino-3-(4-benzyloxyphenyl)-3-hydroxypropioic acid

: 444154-79-4
N,N-[(2S,3R)-2-benzyloxycarbonylamino-3-(4-benzyloxyphenyl)-3-hydroxypropionyl]-β-alanyl-β-alanine methyl ester

Guidance literature:: With dmap; 1-hydroxy-7-aza-benzotriazole; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In dichloromethane; at 20 ℃;
DOI:10.1021/jo0256078

Reference yield: 64.0%

: 444154-77-2
(2S,3R)-2-benzyloxycarbonylamino-3-(4-benzyloxyphenyl)-3-hydroxypropioic acid

: 444154-96-5
N⁵-benzyloxycarbonyl-(N⁵-benzyloxy-N²-benzyloxycarbonyl-N⁵,N-β-alanyl-β-alanyl-N²-methyl-L-ornithyl)-N-[(S)-1-benzyloxy-2-oxo-3-piperidyl]-L-ornithinamide

: N⁵-benzyloxycarbonyl-[N⁵-benzyloxy-N²-benzyloxycarbonyl-N⁵,N,N-[(2S,3R)-2-benzyloxycarbonylamino-3-(4-benzyloxyphenyl)-3-hydroxypropionyl]-β-alanyl-β-alanyl-N²-methyl-L-ornithyl]-N-[(S)-1-benzyloxy-2-oxo-3-piperidyl]-L-ornithinamide

Guidance literature:: With 1-hydroxy-7-aza-benzotriazole; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In dichloromethane; at 20 ℃;
DOI:10.1021/jo0256078