N-[2,4-dimethoxy-5-(2-methoxybenzoylamino)phenyl]-2-methoxyisophthalamic acid

Base Information

Chemical Name:N-[2,4-dimethoxy-5-(2-methoxybenzoylamino)phenyl]-2-methoxyisophthalamic acid
CAS No.:774236-31-6
Molecular Formula:C₂₅H₂₄N₂O₈
Molecular Weight:480.474
Hs Code.:

Synonyms:N-[2,4-dimethoxy-5-(2-methoxybenzoylamino)phenyl]-2-methoxyisophthalamic acid

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Chemical Property of N-[2,4-dimethoxy-5-(2-methoxybenzoylamino)phenyl]-2-methoxyisophthalamic acid

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Technology Process of N-[2,4-dimethoxy-5-(2-methoxybenzoylamino)phenyl]-2-methoxyisophthalamic acid

There total 4 articles about N-[2,4-dimethoxy-5-(2-methoxybenzoylamino)phenyl]-2-methoxyisophthalamic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 774236-30-5
N-[2,4-dimethoxy-5-(2-methoxybenzoylamino)phenyl]-2-methoxyisophthalamic acid methyl ester

: 774236-31-6
N-[2,4-dimethoxy-5-(2-methoxybenzoylamino)phenyl]-2-methoxyisophthalamic acid

Guidance literature:: With lithium hydroxide; In tetrahydrofuran; methanol; at 50 ℃; for 3h;
DOI:10.1021/jo0490705

Reference yield:

: 774236-29-2
N-(5-amino-2,4-dimethoxyphenyl)-2-methoxybenzamide

: 774236-31-6
N-[2,4-dimethoxy-5-(2-methoxybenzoylamino)phenyl]-2-methoxyisophthalamic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / Et₃N / CH₂Cl₂ / 12 h / 20 °C

2: 98 percent / lithium hydroxide hydrate / tetrahydrofuran; methanol / 3 h / 50 °C

With lithium hydroxide; triethylamine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jo0490705

Reference yield:

: 107020-28-0
2-methoxy-3-methoxycarbonylbenzoyl chloride

: 774236-31-6
N-[2,4-dimethoxy-5-(2-methoxybenzoylamino)phenyl]-2-methoxyisophthalamic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / Et₃N / CH₂Cl₂ / 12 h / 20 °C

2: 98 percent / lithium hydroxide hydrate / tetrahydrofuran; methanol / 3 h / 50 °C

With lithium hydroxide; triethylamine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jo0490705