11-(dicyclohexylphosphino)-9-methyl-12-phenyl-9,10-dihydro-9,10-ethenoanthracene

Base Information

Chemical Name:11-(dicyclohexylphosphino)-9-methyl-12-phenyl-9,10-dihydro-9,10-ethenoanthracene
CAS No.:1422448-37-0
Molecular Formula:C₃₅H₃₉P
Molecular Weight:490.668
Hs Code.:

Synonyms:11-(dicyclohexylphosphino)-9-methyl-12-phenyl-9,10-dihydro-9,10-ethenoanthracene

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Chemical Property of 11-(dicyclohexylphosphino)-9-methyl-12-phenyl-9,10-dihydro-9,10-ethenoanthracene

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Technology Process of 11-(dicyclohexylphosphino)-9-methyl-12-phenyl-9,10-dihydro-9,10-ethenoanthracene

There total 3 articles about 11-(dicyclohexylphosphino)-9-methyl-12-phenyl-9,10-dihydro-9,10-ethenoanthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1422448-36-9
11-(dicyclohexylphosphinoyl)-9-methyl-12-phenyl-9,10-dihydro-9,10-ethenoanthracene

: 1422448-37-0
11-(dicyclohexylphosphino)-9-methyl-12-phenyl-9,10-dihydro-9,10-ethenoanthracene

Guidance literature:: With trichlorosilane; triethylamine; In toluene; at 110 ℃; for 72h; Schlenk technique; Inert atmosphere;
DOI:10.1021/om3011992

Reference yield:

: 1166994-71-3
dicyclohexyl(phenylethynyl)phosphine oxide

: 1422448-37-0
11-(dicyclohexylphosphino)-9-methyl-12-phenyl-9,10-dihydro-9,10-ethenoanthracene

Guidance literature:: Multi-step reaction with 2 steps

1: neat (no solvent) / 16 h / 210 - 220 °C / Sealed tube

2: triethylamine; trichlorosilane / toluene / 72 h / 110 °C / Schlenk technique; Inert atmosphere

With trichlorosilane; triethylamine; In toluene; 1: |Diels-Alder Cycloaddition;
DOI:10.1021/om3011992

Reference yield:

: 779-02-2
9-methylanthracene

: 1422448-37-0
11-(dicyclohexylphosphino)-9-methyl-12-phenyl-9,10-dihydro-9,10-ethenoanthracene

Guidance literature:: Multi-step reaction with 2 steps

1: neat (no solvent) / 16 h / 210 - 220 °C / Sealed tube

2: triethylamine; trichlorosilane / toluene / 72 h / 110 °C / Schlenk technique; Inert atmosphere

With trichlorosilane; triethylamine; In toluene; 1: |Diels-Alder Cycloaddition;
DOI:10.1021/om3011992