methyl 3-benzamido-4-O-benzoyl-2,3,6-trideoxy-α-D-erythro-hex-5-enopyranoside

Base Information

Chemical Name:methyl 3-benzamido-4-O-benzoyl-2,3,6-trideoxy-α-D-erythro-hex-5-enopyranoside
CAS No.:92175-37-6
Molecular Formula:C₂₁H₂₁NO₅
Molecular Weight:367.401
Hs Code.:

Synonyms:methyl 3-benzamido-4-O-benzoyl-2,3,6-trideoxy-α-D-erythro-hex-5-enopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 3-benzamido-4-O-benzoyl-2,3,6-trideoxy-α-D-erythro-hex-5-enopyranoside

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Technology Process of methyl 3-benzamido-4-O-benzoyl-2,3,6-trideoxy-α-D-erythro-hex-5-enopyranoside

There total 7 articles about methyl 3-benzamido-4-O-benzoyl-2,3,6-trideoxy-α-D-erythro-hex-5-enopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 92175-36-5
Methyl 3-benzamido-4-O-benzoyl-6-bromo-2,3,6-trideoxy-α-D-ribo-hexopyranoside

: 92175-37-6
methyl 3-benzamido-4-O-benzoyl-2,3,6-trideoxy-α-D-erythro-hex-5-enopyranoside

Guidance literature:: With 1,5-Diazabicyclo[5.4.0]undec-5-ene; In N,N,N,N,N,N-hexamethylphosphoric triamide; for 48h; Ambient temperature;
DOI:10.1016/0008-6215(84)85317-3

Reference yield:

: 20707-11-3
methyl 3-benzamido-4,6-O-benzylidene-2-chloro-2,3-dideoxy-α-D-altropyranoside

: 92175-37-6
methyl 3-benzamido-4-O-benzoyl-2,3,6-trideoxy-α-D-erythro-hex-5-enopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / tri-n-butyltin chloride, sodium borohydride / ethanol / 0.1 h / Heating; Irradiation

2: 76 percent / N-bromosuccinimide, barium carbonate / benzoyl peroxide / CCl₄ / 3 h / Heating

3: 97 percent / 1,5-diazabicyclo<5.4.0>undec-5-ene / hexamethylphosphoric acid triamide / 48 h / Ambient temperature

With sodium tetrahydroborate; N-Bromosuccinimide; tributyltin chloride; barium carbonate; 1,5-Diazabicyclo[5.4.0]undec-5-ene; dibenzoyl peroxide; In tetrachloromethane; N,N,N,N,N,N-hexamethylphosphoric triamide; ethanol;
DOI:10.1016/0008-6215(84)85317-3

Reference yield:

: 16848-75-2
Methyl-3-amino-4,6-O-benzyliden-2,3-didesoxy-α-D-altropyranosid

: 92175-37-6
methyl 3-benzamido-4-O-benzoyl-2,3,6-trideoxy-α-D-erythro-hex-5-enopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 1.) 0 deg C, 2 h; 2.) rt, overnight

2: 76 percent / N-bromosuccinimide, barium carbonate / benzoyl peroxide / CCl₄ / 3 h / Heating

3: 97 percent / 1,5-diazabicyclo<5.4.0>undec-5-ene / hexamethylphosphoric acid triamide / 48 h / Ambient temperature

With pyridine; N-Bromosuccinimide; barium carbonate; 1,5-Diazabicyclo[5.4.0]undec-5-ene; dibenzoyl peroxide; In tetrachloromethane; N,N,N,N,N,N-hexamethylphosphoric triamide;
DOI:10.1016/0008-6215(84)85317-3