Technology Process of methyl 3-benzamido-4-O-benzoyl-2,3,6-trideoxy-α-D-erythro-hex-5-enopyranoside
There total 7 articles about methyl 3-benzamido-4-O-benzoyl-2,3,6-trideoxy-α-D-erythro-hex-5-enopyranoside which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
1,5-Diazabicyclo[5.4.0]undec-5-ene;
In
N,N,N,N,N,N-hexamethylphosphoric triamide;
for 48h;
Ambient temperature;
DOI:10.1016/0008-6215(84)85317-3
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 80 percent / tri-n-butyltin chloride, sodium borohydride / ethanol / 0.1 h / Heating; Irradiation
2: 76 percent / N-bromosuccinimide, barium carbonate / benzoyl peroxide / CCl4 / 3 h / Heating
3: 97 percent / 1,5-diazabicyclo<5.4.0>undec-5-ene / hexamethylphosphoric acid triamide / 48 h / Ambient temperature
With
sodium tetrahydroborate; N-Bromosuccinimide; tributyltin chloride; barium carbonate; 1,5-Diazabicyclo[5.4.0]undec-5-ene;
dibenzoyl peroxide;
In
tetrachloromethane; N,N,N,N,N,N-hexamethylphosphoric triamide; ethanol;
DOI:10.1016/0008-6215(84)85317-3
- Guidance literature:
-
Multi-step reaction with 3 steps
1: pyridine / 1.) 0 deg C, 2 h; 2.) rt, overnight
2: 76 percent / N-bromosuccinimide, barium carbonate / benzoyl peroxide / CCl4 / 3 h / Heating
3: 97 percent / 1,5-diazabicyclo<5.4.0>undec-5-ene / hexamethylphosphoric acid triamide / 48 h / Ambient temperature
With
pyridine; N-Bromosuccinimide; barium carbonate; 1,5-Diazabicyclo[5.4.0]undec-5-ene;
dibenzoyl peroxide;
In
tetrachloromethane; N,N,N,N,N,N-hexamethylphosphoric triamide;
DOI:10.1016/0008-6215(84)85317-3
