C₃₀H₂₃N₃OS₃

Base Information

• Chemical Name: C₃₀H₂₃N₃OS₃
• CAS No.: 1616428-64-8
• Molecular Formula: C₃₀H₂₃N₃OS₃
• Molecular Weight: 537.73
• Mol file: 1616428-64-8.mol

Synonyms:C₃₀H₂₃N₃OS₃

Chemical Property of C₃₀H₂₃N₃OS₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₀H₂₃N₃OS₃

There total 7 articles about C₃₀H₂₃N₃OS₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

5-bromo-5’-methyl-4,4’-bi-(2-phenyl)-thiazole (1616428-63-7) + 2-(4-methoxyphenyl)-5-methyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)thiazole (1616428-62-6) → C30H23N3OS3 (1616428-64-8)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; cesium fluoride; In 1,4-dioxane; Inert atmosphere; Reflux;

DOI:10.1039/c4cc02179g

Reference yield:

2,3-Pentanedione (600-14-6) → C30H23N3OS3 (1616428-64-8)

Guidance literature:

Multi-step reaction with 4 steps

1: bromine / 1.5 h / 20 °C

2: methanol / 0.33 h / 20 °C / Reflux

3: N-Bromosuccinimide / N,N-dimethyl-formamide / 70 °C

4: cesium fluoride; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane / Inert atmosphere; Reflux

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; bromine; cesium fluoride; In 1,4-dioxane; methanol; N,N-dimethyl-formamide;

DOI:10.1039/c4cc02179g

Reference yield:

5-methyl-2-phenyl-4-(2-phenylthiazol-4-yl)thiazole (1616428-67-1) → C30H23N3OS3 (1616428-64-8)

Guidance literature:

Multi-step reaction with 2 steps

1: N-Bromosuccinimide / N,N-dimethyl-formamide / 70 °C

2: cesium fluoride; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane / Inert atmosphere; Reflux

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; cesium fluoride; In 1,4-dioxane; N,N-dimethyl-formamide;

DOI:10.1039/c4cc02179g

upstream raw materials:

1,4-dibromopentane-2,3-dione

5-methyl-2-phenyl-4-(2-phenylthiazol-4-yl)thiazole

5-bromo-5’-methyl-4,4’-bi-(2-phenyl)-thiazole

2-(4-methoxyphenyl)-5-methyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)thiazole

Downstream raw materials:

C₂₉H₂₁N₃OS₃

C₃₂H₂₃N₃OS₃

C₄₁H₄₄N₆O₄S₃Si