4-(5-methylsulfanyl-1,3,4-oxadiazol-2-yl)anilino-4H-1,2,4-triazol-4-yl-aminomethanethione

Base Information

Chemical Name:4-(5-methylsulfanyl-1,3,4-oxadiazol-2-yl)anilino-4H-1,2,4-triazol-4-yl-aminomethanethione
CAS No.:1350301-80-2
Molecular Formula:C₁₂H₁₁N₇OS₂
Molecular Weight:333.398
Hs Code.:

Synonyms:4-(5-methylsulfanyl-1,3,4-oxadiazol-2-yl)anilino-4H-1,2,4-triazol-4-yl-aminomethanethione

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Chemical Property of 4-(5-methylsulfanyl-1,3,4-oxadiazol-2-yl)anilino-4H-1,2,4-triazol-4-yl-aminomethanethione

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Technology Process of 4-(5-methylsulfanyl-1,3,4-oxadiazol-2-yl)anilino-4H-1,2,4-triazol-4-yl-aminomethanethione

There total 2 articles about 4-(5-methylsulfanyl-1,3,4-oxadiazol-2-yl)anilino-4H-1,2,4-triazol-4-yl-aminomethanethione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 584-13-4
4-amino-1,2,4-triazole

: 1350301-74-4
5-(4-isothiocyanatophenyl)-2-methylsulfanyl-1,3,4-oxadiazole

: 1350301-80-2
4-(5-methylsulfanyl-1,3,4-oxadiazol-2-yl)anilino-4H-1,2,4-triazol-4-yl-aminomethanethione

Guidance literature:: In benzene; for 3h; Reflux;
DOI:10.1016/j.bmc.2011.09.038

Reference yield:

: 5-(4-isothiocyanatophenyl)-1,3,4-oxadiazole-2-thiol

: 1350301-80-2
4-(5-methylsulfanyl-1,3,4-oxadiazol-2-yl)anilino-4H-1,2,4-triazol-4-yl-aminomethanethione

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / acetone / 2 h / 20 °C

2: benzene / 3 h / Reflux

With triethylamine; In acetone; benzene;
DOI:10.1016/j.bmc.2011.09.038