N,N’-(1,4-phenylene)dicyanamide

Base Information

• Chemical Name: N,N’-(1,4-phenylene)dicyanamide
• CAS No.: 97954-62-6
• Molecular Formula: C₈H₆N₄
• Molecular Weight: 158.162
• Mol file: 97954-62-6.mol

Synonyms:N,N’-(1,4-phenylene)dicyanamide

Chemical Property of N,N’-(1,4-phenylene)dicyanamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N,N’-(1,4-phenylene)dicyanamide

There total 9 articles about N,N’-(1,4-phenylene)dicyanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

p-phenylenebis-1H-tetrazole (21788-29-4) → N,N’-(1,4-phenylene)dicyanamide (97954-62-6)

Guidance literature:

With potassium hydroxide; In dimethyl sulfoxide; isopropyl alcohol; at 75 - 80 ℃; for 2.5h;

DOI:10.1007/BF00476984

Reference yield: 84.0%

1 ,4-phenylenediisothiocyanate (4044-65-9) → N,N’-(1,4-phenylene)dicyanamide (97954-62-6)

Guidance literature:

With sodium hexamethyldisilazane; In tetrahydrofuran; at 20 ℃; Inert atmosphere;

DOI:10.1016/j.tetlet.2008.08.106

Reference yield: 79.0%

bromocyane (506-68-3) + 1,4-phenylenediamine (106-50-3) → N,N’-(1,4-phenylene)dicyanamide (97954-62-6)

Guidance literature:

With sodium hydrogencarbonate; In water;

upstream raw materials:

N,N'-bis(thiocarbamoyl)-1,4-phenylenediamine

p-phenylenebis-1H-tetrazole

bromocyane

1,4-phenylenediamine

Downstream raw materials:

N,N'-Dicyano-1,4-benzoquinonediimine

N,N'-Dicyano-1,4-benzoquinonediimine

1-(4-bromophenyl)-1H-tetrazol-5-ylamine

N-(4-bromophenyl)-2H-tetrazol-5-amine