2-(benzo[d]thiazol-2-ylsulfonyl)-1-(4-chlorophenyl)-2,2-difluoroethanone

Base Information

Chemical Name:2-(benzo[d]thiazol-2-ylsulfonyl)-1-(4-chlorophenyl)-2,2-difluoroethanone
CAS No.:1241899-82-0
Molecular Formula:C₁₅H₈ClF₂NO₃S₂
Molecular Weight:387.815
Hs Code.:

Synonyms:2-(benzo[d]thiazol-2-ylsulfonyl)-1-(4-chlorophenyl)-2,2-difluoroethanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(benzo[d]thiazol-2-ylsulfonyl)-1-(4-chlorophenyl)-2,2-difluoroethanone

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Technology Process of 2-(benzo[d]thiazol-2-ylsulfonyl)-1-(4-chlorophenyl)-2,2-difluoroethanone

There total 3 articles about 2-(benzo[d]thiazol-2-ylsulfonyl)-1-(4-chlorophenyl)-2,2-difluoroethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 331984-40-8
2-(benzo[d]thiazol-2-ylsulfonyl)-1-(4-chlorophenyl)ethanone

: 1241899-82-0
2-(benzo[d]thiazol-2-ylsulfonyl)-1-(4-chlorophenyl)-2,2-difluoroethanone

Guidance literature:: 2-(benzo[d]thiazol-2-ylsulfonyl)-1-(4-chlorophenyl)ethanone; With sodium carbonate; In acetonitrile; at 20 ℃; Inert atmosphere;

With Selectfluor; In acetonitrile; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.jfluchem.2009.12.022

Reference yield:

: C₁₅H₈ClF₂NOS₂

: 1241899-82-0
2-(benzo[d]thiazol-2-ylsulfonyl)-1-(4-chlorophenyl)-2,2-difluoroethanone

Guidance literature:: With ruthenium trichloride; sodium periodate; In dichloromethane; water; acetonitrile;
DOI:10.1016/j.tetlet.2016.12.070

Reference yield:

: 1338328-40-7
2-bromo-1-(4-chlorophenyl)-2,2-difluoroethan-1-one

: 149-30-4,118090-09-8
2-Mercaptobenzothiazole

: 1241899-82-0
2-(benzo[d]thiazol-2-ylsulfonyl)-1-(4-chlorophenyl)-2,2-difluoroethanone

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / 20 °C

2: sodium periodate; ruthenium trichloride / dichloromethane; water; acetonitrile

With ruthenium trichloride; sodium periodate; triethylamine; In dichloromethane; water; acetonitrile;
DOI:10.1016/j.tetlet.2016.12.070