C₅H₅(CO)((C₆H₅)3P)Fe(COCH₂CH₂NH)⁽¹⁺⁾*PF₆^(1-)=[C₅H₅(CO)((C₆H₅)3P)Fe(COCH₂CH₂NH)]PF₆

Base Information

• Chemical Name: C₅H₅(CO)((C₆H₅)3P)Fe(COCH₂CH₂NH)⁽¹⁺⁾*PF₆^(1-)=[C₅H₅(CO)((C₆H₅)3P)Fe(COCH₂CH₂NH)]PF₆
• CAS No.: 84433-11-4
• Molecular Formula: C₂₇H₂₅FeNO₂P*F₆P
• Molecular Weight: 627.286

Synonyms:C₅H₅(CO)((C₆H₅)3P)Fe(COCH₂CH₂NH)⁽¹⁺⁾*PF₆^(1-)=[C₅H₅(CO)((C₆H₅)3P)Fe(COCH₂CH₂NH)]PF₆

Chemical Property of C₅H₅(CO)((C₆H₅)3P)Fe(COCH₂CH₂NH)⁽¹⁺⁾*PF₆^(1-)=[C₅H₅(CO)((C₆H₅)3P)Fe(COCH₂CH₂NH)]PF₆

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Technology Process of C₅H₅(CO)((C₆H₅)3P)Fe(COCH₂CH₂NH)⁽¹⁺⁾*PF₆^(1-)=[C₅H₅(CO)((C₆H₅)3P)Fe(COCH₂CH₂NH)]PF₆

There total 2 articles about C₅H₅(CO)((C₆H₅)3P)Fe(COCH₂CH₂NH)⁽¹⁺⁾*PF₆^(1-)=[C₅H₅(CO)((C₆H₅)3P)Fe(COCH₂CH₂NH)]PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

potassium hexafluorophosphate (17084-13-8) + ethyleneimine (151-56-4,9002-98-6) + [dicarbonyl(η5-cyclopentadienyl)iron(II)(PPh3)]BF4 → C5H5(CO)((C6H5)3P)Fe(COCH2CH2NH)(1+)*PF6(1-)=[C5H5(CO)((C6H5)3P)Fe(COCH2CH2NH)]PF6 (84433-11-4)

Guidance literature:

With catalyst: (BrCH₂CH₂NH₃)Br; In acetonitrile; stirring mixture of complex and bromide in CH3CN; addn. of aziridine via syringe at 25°c under N2; after 1.5h addn. of further aziridine; after 6h evapn. to dryness (IR); extn. (CH3CN); filtration; treating with KPF6; evapn.; extn. (CH2Cl2); filtration; evapn.; addn. of Et2O; crystn. overnight at -20°C; washing ppt. (Et2O); drying in vac.; elem. anal.;

Reference yield: 70.0%

ethyleneimine (151-56-4,9002-98-6) + (η5-C5H5)Fe(CO)2(triphenylphosphino) hexafluorophosphate → C5H5(CO)((C6H5)3P)Fe(COCH2CH2NH)(1+)*PF6(1-)=[C5H5(CO)((C6H5)3P)Fe(COCH2CH2NH)]PF6 (84433-11-4)

Guidance literature:

With catalyst: Br(CH₂)2NH₃⁽¹⁺⁾*Br^(1-); In acetonitrile; ratio of educts and catalyst: 1:1:1; evapn. in vac. to dryness, extrd. with CH2Cl2, pptd. with ether at -20°C;

upstream raw materials:

ethyleneimine

potassium hexafluorophosphate

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