C₅₅H₄₆N₄Ni

Base Information

Chemical Name:C₅₅H₄₆N₄Ni
CAS No.:1272464-98-8
Molecular Formula:C₅₅H₄₆N₄Ni
Molecular Weight:821.687
Hs Code.:

C<sub>55</sub>H<sub>46</sub>N<sub>4</sub>Ni

Synonyms:C₅₅H₄₆N₄Ni

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Chemical Property of C₅₅H₄₆N₄Ni

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Technology Process of C₅₅H₄₆N₄Ni

There total 3 articles about C₅₅H₄₆N₄Ni which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1272464-96-6
C₅₈H₅₄N₄NiSi

: 1272464-98-8
C₅₅H₄₆N₄Ni

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 - 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ja107753f

Reference yield:

: 1272464-94-4
C₅₃H₄₅IN₄Ni

: 1272464-98-8
C₅₅H₄₆N₄Ni

Guidance literature:: Multi-step reaction with 2 steps

1.1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; triphenyl-arsane; triethylamine / tetrahydrofuran / 0.33 h / 20 °C / Inert atmosphere

1.2: 12 h / 20 °C / Inert atmosphere

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; triphenyl-arsane; tetrabutyl ammonium fluoride; triethylamine; In tetrahydrofuran;
DOI:10.1021/ja107753f

Reference yield:

: 5-(4-iodophenyl)-10,15,20-tris(2,4,6-trimethylphenyl)porphyrin

: 1272464-98-8
C₅₅H₄₆N₄Ni

Guidance literature:: Multi-step reaction with 3 steps

1.1: nickel(II) acetate tetrahydrate; acetic acid / chloroform / 48 h / Reflux; Inert atmosphere

2.1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; triphenyl-arsane; triethylamine / tetrahydrofuran / 0.33 h / 20 °C / Inert atmosphere

2.2: 12 h / 20 °C / Inert atmosphere

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; triphenyl-arsane; tetrabutyl ammonium fluoride; nickel(II) acetate tetrahydrate; acetic acid; triethylamine; In tetrahydrofuran; chloroform;
DOI:10.1021/ja107753f