C₄₇H₆₆BrNO₂₁

Base Information

• Chemical Name: C₄₇H₆₆BrNO₂₁
• CAS No.: 82812-41-7
• Molecular Formula: C₄₇H₆₆BrNO₂₁
• Molecular Weight: 1060.94
• Mol file: 82812-41-7.mol

Synonyms:C₄₇H₆₆BrNO₂₁

Chemical Property of C₄₇H₆₆BrNO₂₁

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₇H₆₆BrNO₂₁

There total 11 articles about C₄₇H₆₆BrNO₂₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

8-(methoxycarbonyl)octyl 2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-<2,4-di-O-acetyl-3-O-(2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl)-α-L-rhamnopyranosyl>-α-D-glucopyranoside (82812-33-7) → C47H66BrNO21 (82812-41-7)

Guidance literature:

With N-Bromosuccinimide; In tetrachloromethane; for 0.0833333h; Heating; Irradiation;

DOI:10.1016/S0008-6215(82)80027-X

Reference yield:

methyl 9-hydroxynonanoate (34957-73-8) → C47H66BrNO21 (82812-41-7)

Guidance literature:

Multi-step reaction with 9 steps

1: 90 percent / Hg(CN)2 / benzene / 25 °C

2: 60 percent / ZnCl₂ / not given / 130 °C

3: 80 percent / NaOMe / methanol

4: 90 percent / TsOH / 25 °C

5: Hg(CN)2 / benzene; acetonitrile / 50 °C

6: 96 percent / NaOMe / methanol

7: 63 percent / Hg(CN)2 / benzene; acetonitrile / 30 °C

9: 88 percent / N-bromosuccinimide / CCl₄ / 0.08 h / Heating; Irradiation

With N-Bromosuccinimide; sodium methylate; mercury(II) cyanide; toluene-4-sulfonic acid; zinc(II) chloride; In methanol; tetrachloromethane; acetonitrile; benzene;

DOI:10.1016/S0008-6215(82)80027-X

Reference yield:

benzaldehyde dimethyl acetal (1125-88-8) → C47H66BrNO21 (82812-41-7)

Guidance literature:

Multi-step reaction with 6 steps

1: 90 percent / TsOH / 25 °C

2: Hg(CN)2 / benzene; acetonitrile / 50 °C

3: 96 percent / NaOMe / methanol

4: 63 percent / Hg(CN)2 / benzene; acetonitrile / 30 °C

6: 88 percent / N-bromosuccinimide / CCl₄ / 0.08 h / Heating; Irradiation

With N-Bromosuccinimide; sodium methylate; mercury(II) cyanide; toluene-4-sulfonic acid; In methanol; tetrachloromethane; acetonitrile; benzene;

DOI:10.1016/S0008-6215(82)80027-X

upstream raw materials:

8-(methoxycarbonyl)octyl 2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-<2,4-di-O-acetyl-3-O-(2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl)-α-L-rhamnopyranosyl>-α-D-glucopyranoside

methyl 9-hydroxynonanoate

benzaldehyde dimethyl acetal

(Methoxycarbonyl)octyl 2-acetamido-3,4,6-tri-O-acetyl-β-D-glucopyranoside

Downstream raw materials:

C₄₇H₆₇NO₂₁