2',5-dichloro-2-<3-(aminomethyl)-5-methyl-4H-1,2,4-triazol-4-yl>benzophenone dihydrobromide

Base Information

Chemical Name:2',5-dichloro-2-<3-(aminomethyl)-5-methyl-4H-1,2,4-triazol-4-yl>benzophenone dihydrobromide
CAS No.:64194-71-4
Molecular Formula:2BrH*C₁₇H₁₄Cl₂N₄O
Molecular Weight:523.054
Hs Code.:

Synonyms:2',5-dichloro-2-<3-(aminomethyl)-5-methyl-4H-1,2,4-triazol-4-yl>benzophenone dihydrobromide

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Chemical Property of 2',5-dichloro-2-<3-(aminomethyl)-5-methyl-4H-1,2,4-triazol-4-yl>benzophenone dihydrobromide

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Technology Process of 2',5-dichloro-2-<3-(aminomethyl)-5-methyl-4H-1,2,4-triazol-4-yl>benzophenone dihydrobromide

There total 9 articles about 2',5-dichloro-2-<3-(aminomethyl)-5-methyl-4H-1,2,4-triazol-4-yl>benzophenone dihydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 83520-17-6
2',5-dichloro-2-<3-<<(benzyloxycarbonyl)amino>methyl>-5-methyl-4H-1,2,4-triazol-4-yl>benzophenone

: 64194-71-4
2',5-dichloro-2-<3-(aminomethyl)-5-methyl-4H-1,2,4-triazol-4-yl>benzophenone dihydrobromide

Guidance literature:: With hydrogen bromide; acetic acid; In acetonitrile; 1.) RT, 1.5 h, 2.) reflux, 1 h;
DOI:10.1021/jm00354a015

Reference yield:

: 2958-36-3,53960-29-5
(2-amino-5-chloro-phenyl)-(2-chloro-phenyl)-methanone

: 64194-71-4
2',5-dichloro-2-<3-(aminomethyl)-5-methyl-4H-1,2,4-triazol-4-yl>benzophenone dihydrobromide

Guidance literature:: Multi-step reaction with 4 steps

2: 17 percent / AcOH / ethanol / 6 h / Ambient temperature

4: 99 percent / 30percent HBr, AcOH / acetonitrile / 1.) RT, 1.5 h, 2.) reflux, 1 h

With hydrogen bromide; acetic acid; In ethanol; acetonitrile;
DOI:10.1021/jm00354a015

Reference yield:

: 83520-07-4
2-thioacetamido-2',5-dichlorobenzophenone

: 64194-71-4
2',5-dichloro-2-<3-(aminomethyl)-5-methyl-4H-1,2,4-triazol-4-yl>benzophenone dihydrobromide

Guidance literature:: Multi-step reaction with 3 steps

1: 33 percent / AcOH / ethanol / 14 h / Ambient temperature

3: 99 percent / 30percent HBr, AcOH / acetonitrile / 1.) RT, 1.5 h, 2.) reflux, 1 h

With hydrogen bromide; acetic acid; In ethanol; acetonitrile;
DOI:10.1021/jm00354a015