1-(21,43-bis((octadec-9-enoyloxy)methyl)-18,23,40,45,62,68-hexaoxo-19,22,41,44,63,67-hexaoxapentaoctaconta-9,31,53,76-tetraen-65-yl) 18-(1,3-bis(octadec-9-enoyloxy)propan-2-yl) octadec-9-enedioate

Base Information

• Chemical Name: 1-(21,43-bis((octadec-9-enoyloxy)methyl)-18,23,40,45,62,68-hexaoxo-19,22,41,44,63,67-hexaoxapentaoctaconta-9,31,53,76-tetraen-65-yl) 18-(1,3-bis(octadec-9-enoyloxy)propan-2-yl) octadec-9-enedioate
• CAS No.: 1437306-87-0
• Molecular Formula: C₁₇₄H₃₀₈O₂₄
• Molecular Weight: 2784.35

Synonyms:1-(21,43-bis((octadec-9-enoyloxy)methyl)-18,23,40,45,62,68-hexaoxo-19,22,41,44,63,67-hexaoxapentaoctaconta-9,31,53,76-tetraen-65-yl) 18-(1,3-bis(octadec-9-enoyloxy)propan-2-yl) octadec-9-enedioate

Chemical Property of 1-(21,43-bis((octadec-9-enoyloxy)methyl)-18,23,40,45,62,68-hexaoxo-19,22,41,44,63,67-hexaoxapentaoctaconta-9,31,53,76-tetraen-65-yl) 18-(1,3-bis(octadec-9-enoyloxy)propan-2-yl) octadec-9-enedioate

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Technology Process of 1-(21,43-bis((octadec-9-enoyloxy)methyl)-18,23,40,45,62,68-hexaoxo-19,22,41,44,63,67-hexaoxapentaoctaconta-9,31,53,76-tetraen-65-yl) 18-(1,3-bis(octadec-9-enoyloxy)propan-2-yl) octadec-9-enedioate

There total 1 articles about 1-(21,43-bis((octadec-9-enoyloxy)methyl)-18,23,40,45,62,68-hexaoxo-19,22,41,44,63,67-hexaoxapentaoctaconta-9,31,53,76-tetraen-65-yl) 18-(1,3-bis(octadec-9-enoyloxy)propan-2-yl) octadec-9-enedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.1%

trioleoylglycerol (122-32-7) → octadec-9-enoic acid propane-1,2,3-triyl ester (6915-08-8,69466-36-0) + 18-bis(1,3-bis(octadec-9-enoyloxy)propan-2-yl)-1,1-3-(octadec-9-enoyloxy)propane-1,2-diyl dioctadec-9-enedioate (1437306-86-9) + 1-(21,43-bis((octadec-9-enoyloxy)methyl)-18,23,40,45,62,68-hexaoxo-19,22,41,44,63,67-hexaoxapentaoctaconta-9,31,53,76-tetraen-65-yl) 18-(1,3-bis(octadec-9-enoyloxy)propan-2-yl) octadec-9-enedioate (1437306-87-0) + 1-(21,42-bis((octadec-9-enoyloxy)methyl)-18,23,40,45,62,68-hexaoxo-19,22,41,44,63,67-hexaoxapentaoctaconta-9,31,53,76-tetraen-65-yl)18-(2-(18-(1,3-bis(octadec-9-enoyloxy)propan-2-yloxy)-18-oxooctadec-9-enoyloxy)-3-(octadec-9-enoyloxy)propyl) octadec-9-enedioate + bis(1,3-bis(octadec-9-enoyloxy)propan-2-yl) octadec-9-enedioate (1437306-85-8)

Guidance literature:

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In neat (no solvent); at 38 ℃; for 6h; Overall yield = 21.4 %; Inert atmosphere;

DOI:10.1007/s11746-012-2106-y

upstream raw materials:

trioleoylglycerol

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