iso-butyl sidechain acid

Base Information

Chemical Name:iso-butyl sidechain acid
CAS No.:849213-13-4
Molecular Formula:C₂₃H₂₇NO₆
Molecular Weight:413.47
Hs Code.:

Synonyms:iso-butyl sidechain acid

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Chemical Property of iso-butyl sidechain acid

Chemical Property:

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Technology Process of iso-butyl sidechain acid

There total 5 articles about iso-butyl sidechain acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 849213-12-3
3-N,2-O-anisaldehyde acetal-3-N-Cbz-5-methyl hexanoyl methyl ester

: 849213-13-4
iso-butyl sidechain acid

Guidance literature:: 3-N,2-O-anisaldehyde acetal-3-N-Cbz-5-methyl hexanoyl methyl ester; With lithium hydroxide; water; In ethanol; at 20 ℃; for 4.83333h;

With hydrogenchloride; In water; pH=1;

Reference yield:

: 2186-92-7
p-Anisaldehyde dimethyl acetal

: 849213-13-4
iso-butyl sidechain acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: toluene-4-sulfonic acid / toluene / 2.5 h / Heating / reflux

2.1: lithium hydroxide; water / ethanol / 4.83 h / 20 °C

2.2: pH 1

With lithium hydroxide; water; toluene-4-sulfonic acid; In ethanol; toluene;

Reference yield:

: 318464-20-9
(2R,3S)-3-amino-2-hydroxy-5-methylhexanoic acid

: 849213-13-4
iso-butyl sidechain acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: thionyl chloride / 4.5 h / 0 °C

1.2: 3 h / pH 8.5

2.1: toluene-4-sulfonic acid / toluene / 2.5 h / Heating / reflux

3.1: lithium hydroxide; water / ethanol / 4.83 h / 20 °C

3.2: pH 1

With lithium hydroxide; thionyl chloride; water; toluene-4-sulfonic acid; In ethanol; toluene;