3-(4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalen-6-yl)phenylamine hydrochloride

Base Information

Chemical Name:3-(4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalen-6-yl)phenylamine hydrochloride
CAS No.:1469857-69-9
Molecular Formula:C₁₄H₁₁N₃S*ClH
Molecular Weight:289.788
Hs Code.:

Synonyms:3-(4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalen-6-yl)phenylamine hydrochloride

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Chemical Property of 3-(4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalen-6-yl)phenylamine hydrochloride

Chemical Property:

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Technology Process of 3-(4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalen-6-yl)phenylamine hydrochloride

There total 6 articles about 3-(4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalen-6-yl)phenylamine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1469858-41-0
N-{3-[4-(2-trimethylsilanylethoxymethyl)-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalen-6-yl]phenyl}acetamide

: 1469857-69-9
3-(4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalen-6-yl)phenylamine hydrochloride

Guidance literature:: With hydrogenchloride; In methanol; at 100 ℃; for 4h;

Reference yield:

: 82723-17-9
3-bromobenzoic acid phenyl ester

: 1469857-69-9
3-(4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalen-6-yl)phenylamine hydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydride / mineral oil; tetrahydrofuran / 8 h / 100 °C

2: hydrazine hydrate; acetic acid / ethanol / 4 h / 100 °C / Inert atmosphere

3: sodium hydride / mineral oil; tetrahydrofuran / 2.5 h / 0 - 80 °C

4: caesium carbonate; palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / 1,4-dioxane / 8 h / 100 °C

5: hydrogenchloride / methanol; water / 4 h / 100 °C

With hydrogenchloride; palladium diacetate; sodium hydride; caesium carbonate; hydrazine hydrate; acetic acid; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; water; mineral oil;

Reference yield:

: 1469858-35-2
5-(3-bromobenzoyl)-5,6-dihydrocyclopenta[b]thiophen-4-one

: 1469857-69-9
3-(4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalen-6-yl)phenylamine hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: hydrazine hydrate; acetic acid / ethanol / 4 h / 100 °C / Inert atmosphere

2: sodium hydride / mineral oil; tetrahydrofuran / 2.5 h / 0 - 80 °C

3: caesium carbonate; palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / 1,4-dioxane / 8 h / 100 °C

4: hydrogenchloride / methanol; water / 4 h / 100 °C

With hydrogenchloride; palladium diacetate; sodium hydride; caesium carbonate; hydrazine hydrate; acetic acid; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; water; mineral oil;