C₃₈H₅₁NO₆Si₂

Base Information

Chemical Name:C₃₈H₅₁NO₆Si₂
CAS No.:1295471-53-2
Molecular Formula:C₃₈H₅₁NO₆Si₂
Molecular Weight:673.997
Hs Code.:

C<sub>38</sub>H<sub>51</sub>NO<sub>6</sub>Si<sub>2</sub>

Synonyms:C₃₈H₅₁NO₆Si₂

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Chemical Property of C₃₈H₅₁NO₆Si₂

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Technology Process of C₃₈H₅₁NO₆Si₂

There total 4 articles about C₃₈H₅₁NO₆Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1295471-03-2
C₃₉H₅₃NO₅Si₂

: 1295471-53-2
C₃₈H₅₁NO₆Si₂

Guidance literature:: C₃₉H₅₃NO₅Si₂; With ozone; In dichloromethane; at -78 ℃;

With dimethylsulfide; In dichloromethane; at -78 - 20 ℃;
DOI:10.1002/anie.201008079

Reference yield:

: 1295471-52-1
C₃₉H₅₅NO₅Si₂

: 1295471-53-2
C₃₈H₅₁NO₆Si₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.5 h / -78 °C / Inert atmosphere

1.2: 1 h / -78 - 0 °C

2.1: ozone / dichloromethane / -78 °C

2.2: -78 - 20 °C

With oxalyl dichloride; ozone; dimethyl sulfoxide; In dichloromethane;
DOI:10.1002/anie.201008079

Reference yield:

: L-threonine

: 1295471-53-2
C₃₈H₅₁NO₆Si₂

Guidance literature:: Multi-step reaction with 7 steps

1: thionyl chloride / acetonitrile / 0 - 20 °C

2: lithium hexamethyldisilazane / tetrahydrofuran / -78 °C

3: 2,6-dimethylpyridine / dichloromethane / 0 - 20 °C

4: diisobutylaluminium hydride / dichloromethane / -78 °C

5: methylmagnesium bromide / diethyl ether / 0 °C

6: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / -78 °C

7: ozone / dichloromethane / -78 °C

With 2,6-dimethylpyridine; thionyl chloride; oxalyl dichloride; methylmagnesium bromide; diisobutylaluminium hydride; ozone; dimethyl sulfoxide; triethylamine; lithium hexamethyldisilazane; In tetrahydrofuran; diethyl ether; dichloromethane; acetonitrile;
DOI:10.1021/jo301638z