5,6,7,8-tetrahydro-10,11-dimethoxy-6-methyl-3-phenyl-4H-isoxazolo<4,5-f><3>benzazonine

Base Information

Chemical Name:5,6,7,8-tetrahydro-10,11-dimethoxy-6-methyl-3-phenyl-4H-isoxazolo<4,5-f><3>benzazonine
CAS No.:123420-59-7
Molecular Formula:C₂₂H₂₄N₂O₃
Molecular Weight:364.444
Hs Code.:

Synonyms:5,6,7,8-tetrahydro-10,11-dimethoxy-6-methyl-3-phenyl-4H-isoxazolo<4,5-f><3>benzazonine

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Chemical Property of 5,6,7,8-tetrahydro-10,11-dimethoxy-6-methyl-3-phenyl-4H-isoxazolo<4,5-f><3>benzazonine

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Technology Process of 5,6,7,8-tetrahydro-10,11-dimethoxy-6-methyl-3-phenyl-4H-isoxazolo<4,5-f><3>benzazonine

There total 4 articles about 5,6,7,8-tetrahydro-10,11-dimethoxy-6-methyl-3-phenyl-4H-isoxazolo<4,5-f><3>benzazonine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 133964-06-4
(3RS,9bRS,12aRS)-1,4,5,12a-tetrahydro-7,8-dimethoxy-3-methyl-12-phenyl-2H-isoxazolo<5',4':2,3>pyrrolo<2,1-a>isoquinolinium iodide

: 123420-59-7
5,6,7,8-tetrahydro-10,11-dimethoxy-6-methyl-3-phenyl-4H-isoxazolo<4,5-f><3>benzazonine

Guidance literature:: With sodium methylate; In methanol; at 25 ℃; for 2h;
DOI:10.1021/jo00015a025

Reference yield:

: 123420-50-8
8,9-dimethoxy-2,3,5,6-tetrahydro-1H-pyrrolo[2,1-a]isoquinolinium; bromide

: 123420-59-7
5,6,7,8-tetrahydro-10,11-dimethoxy-6-methyl-3-phenyl-4H-isoxazolo<4,5-f><3>benzazonine

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / Et₃N / CHCl₃ / 1) ice bath, 0.5 h, 2) 25 deg C, 1 h

2: 94 percent / 8 h / Heating

3: 72 percent / NaOMe / methanol / 2 h / 25 °C

With sodium methylate; triethylamine; In methanol; chloroform;
DOI:10.1021/jo00015a025

Reference yield:

: 133964-05-3
(9bRS,12aRS)-1,4,5,12a-tetrahydro-7,8-dimethoxy-12-phenyl-2H-isoxazolo<5',4':2,3>pyrrolo<2,1-a>isoquinoline

: 123420-59-7
5,6,7,8-tetrahydro-10,11-dimethoxy-6-methyl-3-phenyl-4H-isoxazolo<4,5-f><3>benzazonine

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / 8 h / Heating

2: 72 percent / NaOMe / methanol / 2 h / 25 °C

With sodium methylate; In methanol;
DOI:10.1021/jo00015a025