4-(3',5'-Di(3'',5''dibenzyloxy)benzyloxy)benzyloxyphthalonitrile

Base Information

• Chemical Name: 4-(3',5'-Di(3'',5''dibenzyloxy)benzyloxy)benzyloxyphthalonitrile
• CAS No.: 207562-27-4
• Molecular Formula: C₅₇H₄₆N₂O₇
• Molecular Weight: 871.001
• Mol file: 207562-27-4.mol

Synonyms:4-(3',5'-Di(3'',5''dibenzyloxy)benzyloxy)benzyloxyphthalonitrile

Chemical Property of 4-(3',5'-Di(3'',5''dibenzyloxy)benzyloxy)benzyloxyphthalonitrile

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-(3',5'-Di(3'',5''dibenzyloxy)benzyloxy)benzyloxyphthalonitrile

There total 1 articles about 4-(3',5'-Di(3'',5''dibenzyloxy)benzyloxy)benzyloxyphthalonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

4-Nitrophthalonitrile (31643-49-9) + [3,5-Bis-(3,5-bis-benzyloxy-benzyloxy)-phenyl]-methanol (129536-40-9) → 4-(3',5'-Di(3'',5''dibenzyloxy)benzyloxy)benzyloxyphthalonitrile (207562-27-4)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 48h;

DOI:10.1002/1521-3765(20001215)6:24<4630::AID-CHEM4630>3.0.CO;2-F

Reference yield: 32.0%

4,5-Bis(1,4,7-trioxaoctyl)phthalonitrile (178813-97-3) + 4-(3',5'-Di(3'',5''dibenzyloxy)benzyloxy)benzyloxyphthalonitrile (207562-27-4) → 2-(3',5'-Di(3'',5''-dibenzyloxy)benzyloxy)benzyloxy-9,10,16,17,23,24-hexa(1,4,7-trioxaoctyl)phthalocyanine

Guidance literature:

With pentan-1-ol; lithium hydride; at 135 ℃; for 6h;

DOI:10.1002/1521-3765(20001215)6:24<4630::AID-CHEM4630>3.0.CO;2-F

Reference yield:

4,5-Bis(1,4,7-trioxaoctyl)phthalonitrile (178813-97-3) + 4-(3',5'-Di(3'',5''dibenzyloxy)benzyloxy)benzyloxyphthalonitrile (207562-27-4) → 2-(3',5'-Di(3'',5''-dibenzyloxy)benzyloxy)benzyloxy-9,10,16,17,23,24-hexa(1,4,7-trioxaoctyl)phthalocyanine + 2,3,9,10,16,17,23,24-octakis(3,6-dioxaheptyloxy)phthalocyanine

Guidance literature:

With C₅H₁₁OLi; In pentan-1-ol; at 135 ℃;

DOI:10.1039/a801799i

upstream raw materials:

4-Nitrophthalonitrile

[3,5-Bis-(3,5-bis-benzyloxy-benzyloxy)-phenyl]-methanol

Refernces

• 1、 Brewis, Matthew,Clarkson, Guy J.,Helliwell, Madeleine,Holder, Andrea M.,McKeown, Neil B.. "The synthesis and glass-forming properties of phthalocyanine-containing poly(aryl ether) dendrimers". . p. 4630 - 4636. Retrieved 2007/10/03.