N-{N-[(3R)-15-methyl-3-(13-methyltetradecanoyloxy)hexadecanoyl]glycyl}-D-serine benzyl ester

Base Information

Chemical Name:N-{N-[(3R)-15-methyl-3-(13-methyltetradecanoyloxy)hexadecanoyl]glycyl}-D-serine benzyl ester
CAS No.:214406-48-1
Molecular Formula:C₄₄H₇₆N₂O₇
Molecular Weight:745.097
Hs Code.:

Synonyms:N-{N-[(3R)-15-methyl-3-(13-methyltetradecanoyloxy)hexadecanoyl]glycyl}-D-serine benzyl ester

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Chemical Property of N-{N-[(3R)-15-methyl-3-(13-methyltetradecanoyloxy)hexadecanoyl]glycyl}-D-serine benzyl ester

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Technology Process of N-{N-[(3R)-15-methyl-3-(13-methyltetradecanoyloxy)hexadecanoyl]glycyl}-D-serine benzyl ester

There total 9 articles about N-{N-[(3R)-15-methyl-3-(13-methyltetradecanoyloxy)hexadecanoyl]glycyl}-D-serine benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 133099-79-3
D-serine benzyl ester

: 103196-73-2
(3R)-N-<3-(13'-methyltetradecanoyloxy)-15-methylhexadecanoyl>glycine

: 214406-48-1
N-{N-[(3R)-15-methyl-3-(13-methyltetradecanoyloxy)hexadecanoyl]glycyl}-D-serine benzyl ester

Guidance literature:: With dicyclohexyl-carbodiimide; In dichloromethane; for 2h; Ambient temperature;
DOI:10.1016/S0040-4020(98)83044-5

Reference yield:

: 178860-78-1
(3R)-15-methyl-3-(13-methyltetradecanoyloxy)hexadecanoic acid

: 214406-48-1
N-{N-[(3R)-15-methyl-3-(13-methyltetradecanoyloxy)hexadecanoyl]glycyl}-D-serine benzyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: oxalyl chloride / CH₂Cl₂ / 1 h / Ambient temperature

2: Et₃N / CH₂Cl₂ / 1 h / 0 - 5 °C

3: 98 percent / H₂ / Pd/C / ethyl acetate / 2 h / Ambient temperature

4: 82 percent / DCC / CH₂Cl₂ / 2 h / Ambient temperature

With oxalyl dichloride; hydrogen; triethylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In dichloromethane; ethyl acetate;
DOI:10.1016/S0040-4020(98)83044-5

Reference yield:

: 13-Methyl-tetradecanoic acid (R)-1-chlorocarbonylmethyl-13-methyl-tetradecyl ester

: 214406-48-1
N-{N-[(3R)-15-methyl-3-(13-methyltetradecanoyloxy)hexadecanoyl]glycyl}-D-serine benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N / CH₂Cl₂ / 1 h / 0 - 5 °C

2: 98 percent / H₂ / Pd/C / ethyl acetate / 2 h / Ambient temperature

3: 82 percent / DCC / CH₂Cl₂ / 2 h / Ambient temperature

With hydrogen; triethylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In dichloromethane; ethyl acetate;
DOI:10.1016/S0040-4020(98)83044-5