exo,exo-2,4-diphenyl-9,10-diazatetracyclo[3.3.2.0^2.4.0^6.8]dec-9-ene-1,5-dicarbonitrile

Base Information

• Chemical Name: exo,exo-2,4-diphenyl-9,10-diazatetracyclo[3.3.2.0^2.4.0^6.8]dec-9-ene-1,5-dicarbonitrile
• CAS No.: 69901-15-1
• Molecular Formula: C₂₂H₁₆N₄
• Molecular Weight: 336.396

Synonyms:exo,exo-2,4-diphenyl-9,10-diazatetracyclo[3.3.2.0^2.4.0^6.8]dec-9-ene-1,5-dicarbonitrile

Chemical Property of exo,exo-2,4-diphenyl-9,10-diazatetracyclo[3.3.2.0^2.4.0^6.8]dec-9-ene-1,5-dicarbonitrile

Chemical Property:

Purity/Quality:

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Technology Process of exo,exo-2,4-diphenyl-9,10-diazatetracyclo[3.3.2.0^2.4.0^6.8]dec-9-ene-1,5-dicarbonitrile

There total 5 articles about exo,exo-2,4-diphenyl-9,10-diazatetracyclo[3.3.2.0^2.4.0^6.8]dec-9-ene-1,5-dicarbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 9.0%

C22H20N4O2 → exo,exo-2,4-diphenyl-9,10-diazatetracyclo[3.3.2.02.4.06.8]dec-9-ene-1,5-dicarbonitrile (69901-15-1)

Guidance literature:

With trichlorophosphate; In 1,2-dichloro-ethane; for 48h; Heating;

DOI:10.1002/1099-0690(200107)2001:14<2639::aid-ejoc2639>3.0.co;2-0

Reference yield:

1,2-Diphenylcyclopropen (24168-52-3) → exo,exo-2,4-diphenyl-9,10-diazatetracyclo[3.3.2.02.4.06.8]dec-9-ene-1,5-dicarbonitrile (69901-15-1)

Guidance literature:

Multi-step reaction with 4 steps

1.1: 63 percent / CH₂Cl₂ / 40 h / Heating

2.1: 98 percent / KOH / aq. methanol

3.1: SOCl₂ / 2 h / 20 °C

3.2: 77 percent / conc. NH₃ / acetone

4.1: 9 percent / POCl₃ / 1,2-dichloro-ethane / 48 h / Heating

With potassium hydroxide; thionyl chloride; trichlorophosphate; In methanol; dichloromethane; 1,2-dichloro-ethane;

DOI:10.1002/1099-0690(200107)2001:14<2639::aid-ejoc2639>3.0.co;2-0

Reference yield:

Diazanorcaradien (27666-78-0) → exo,exo-2,4-diphenyl-9,10-diazatetracyclo[3.3.2.02.4.06.8]dec-9-ene-1,5-dicarbonitrile (69901-15-1)

Guidance literature:

Multi-step reaction with 4 steps

1.1: 63 percent / CH₂Cl₂ / 40 h / Heating

2.1: 98 percent / KOH / aq. methanol

3.1: SOCl₂ / 2 h / 20 °C

3.2: 77 percent / conc. NH₃ / acetone

4.1: 9 percent / POCl₃ / 1,2-dichloro-ethane / 48 h / Heating

With potassium hydroxide; thionyl chloride; trichlorophosphate; In methanol; dichloromethane; 1,2-dichloro-ethane;

DOI:10.1002/1099-0690(200107)2001:14<2639::aid-ejoc2639>3.0.co;2-0

upstream raw materials:

1,2-Diphenylcyclopropen

Diazanorcaradien

dimethyl exo,exo-2,4-diphenyl-9,10-diazatetracyclo[3.3.2.0^2.4.0^6.8]dec-9-ene-1,5-dicarboxylate

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