phenyl(o-trifluoromethylphenyl)diazomethane

Base Information

Chemical Name:phenyl(o-trifluoromethylphenyl)diazomethane
CAS No.:60664-80-4
Molecular Formula:C₁₄H₉F₃N₂
Molecular Weight:262.234
Hs Code.:

Synonyms:phenyl(o-trifluoromethylphenyl)diazomethane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenyl(o-trifluoromethylphenyl)diazomethane

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Technology Process of phenyl(o-trifluoromethylphenyl)diazomethane

There total 2 articles about phenyl(o-trifluoromethylphenyl)diazomethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 60664-68-8
1-(trifluoromethyl)benzophenone hydrazone

: 60664-80-4
phenyl(o-trifluoromethylphenyl)diazomethane

Guidance literature:: With potassium hydroxide; sodium sulfate; mercury(II) oxide; In diethyl ether; ethanol; for 24h;
DOI:10.1021/j100172a033

Reference yield:

: 727-99-1
2-trifluoromethylbenzophenone

: 60664-80-4
phenyl(o-trifluoromethylphenyl)diazomethane

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / hydrazine / ethanol / Heating

2: 77 percent / mercuric oxide, Na₂SO₄, KOH / ethanol; diethyl ether / 24 h

With potassium hydroxide; sodium sulfate; mercury(II) oxide; hydrazine; In diethyl ether; ethanol;
DOI:10.1021/j100172a033

Reference yield:

: 75-22-9
trimethylamine-borane

: 60664-80-4
phenyl(o-trifluoromethylphenyl)diazomethane

: (-)-trimethylamine-(phenyl(2-(trifluoromethyl)phenyl)methyl)borane

Guidance literature:: With Rh₂[(S)-TBPTTL]₄; In toluene; at -40 ℃; enantioselective reaction; Inert atmosphere; Schlenk technique;
DOI:10.1002/anie.202109447