potassium N-furfuryl-4-(N-methylanilino)-5-(dimethylsulfamoyl)orthanilate

Base Information

Chemical Name:potassium N-furfuryl-4-(N-methylanilino)-5-(dimethylsulfamoyl)orthanilate
CAS No.:85958-75-4
Molecular Formula:C₂₀H₂₂N₃O₆S₂*K
Molecular Weight:503.641
Hs Code.:

Synonyms:potassium N-furfuryl-4-(N-methylanilino)-5-(dimethylsulfamoyl)orthanilate

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Chemical Property of potassium N-furfuryl-4-(N-methylanilino)-5-(dimethylsulfamoyl)orthanilate

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Technology Process of potassium N-furfuryl-4-(N-methylanilino)-5-(dimethylsulfamoyl)orthanilate

There total 7 articles about potassium N-furfuryl-4-(N-methylanilino)-5-(dimethylsulfamoyl)orthanilate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 617-89-0
furan-2-ylmethanamine

: 85958-75-4
potassium N-furfuryl-4-(N-methylanilino)-5-(dimethylsulfamoyl)orthanilate

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / 2.5 h / 125 °C

2: 2.4 g / K₃CO₃ / N,N-dimethyl-acetamide / 1 h / 70 °C

3: 1.) H₂, aq. NH₃, 2.) aq. KCl / 1.) Pd/C / 1.) THF, 20 deg C, 0.1 bar

With ammonium hydroxide; potassium chloride; hydrogen; potassium carbonate; palladium on activated charcoal; In N,N-dimethyl acetamide;
DOI:10.1021/jm00362a017

Reference yield:

: 61791-73-9
4,6-dichlorobenzene-1,3-disulfonyl chloride

: 85958-75-4
potassium N-furfuryl-4-(N-methylanilino)-5-(dimethylsulfamoyl)orthanilate

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) NH₃ / 1.) THF, 5-10 deg C, 2 h, 2.) MeOH, a) reflux, 10 min, b) RT, overnight

2: 53 percent / 6 h / 140 °C

3: 86 percent / 2.5 h / 125 °C

4: 2.4 g / K₃CO₃ / N,N-dimethyl-acetamide / 1 h / 70 °C

5: 1.) H₂, aq. NH₃, 2.) aq. KCl / 1.) Pd/C / 1.) THF, 20 deg C, 0.1 bar

With ammonium hydroxide; potassium chloride; ammonia; hydrogen; potassium carbonate; palladium on activated charcoal; In N,N-dimethyl acetamide;
DOI:10.1021/jm00362a017

Reference yield:

: 80289-32-3
phenyl 2,4-dichloro-5-sulfamoylbenzenesulfonate

: 85958-75-4
potassium N-furfuryl-4-(N-methylanilino)-5-(dimethylsulfamoyl)orthanilate

Guidance literature:: Multi-step reaction with 4 steps

1: 53 percent / 6 h / 140 °C

2: 86 percent / 2.5 h / 125 °C

3: 2.4 g / K₃CO₃ / N,N-dimethyl-acetamide / 1 h / 70 °C

4: 1.) H₂, aq. NH₃, 2.) aq. KCl / 1.) Pd/C / 1.) THF, 20 deg C, 0.1 bar

With ammonium hydroxide; potassium chloride; hydrogen; potassium carbonate; palladium on activated charcoal; In N,N-dimethyl acetamide;
DOI:10.1021/jm00362a017