Technology Process of C18H20BNO4*ClH
There total 6 articles about C18H20BNO4*ClH which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium tris(acetoxy)borohydride; orthoformic acid triethyl ester;
In
ethanol; dichloromethane;
at 20 ℃;
for 1h;
DOI:10.1016/j.bmcl.2013.01.072
- Guidance literature:
-
Multi-step reaction with 5 steps
1: potassium carbonate / N,N-dimethyl-formamide / 80 °C
2: potassium acetate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2 / 1,4-dioxane / 90 °C
3: sodium tetrahydroborate / methanol / 1 h / 0 - 20 °C
4: hydrogenchloride / water
5: sodium tris(acetoxy)borohydride; orthoformic acid triethyl ester / ethanol; dichloromethane / 1 h / 20 °C
With
hydrogenchloride; sodium tetrahydroborate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate; sodium tris(acetoxy)borohydride; potassium carbonate; orthoformic acid triethyl ester;
In
1,4-dioxane; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
2: |Miyaura Borylation Reaction;
DOI:10.1016/j.bmcl.2013.01.072
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium tetrahydroborate / methanol / 1 h / 0 - 20 °C
2: hydrogenchloride / water
3: sodium tris(acetoxy)borohydride; orthoformic acid triethyl ester / ethanol; dichloromethane / 1 h / 20 °C
With
hydrogenchloride; sodium tetrahydroborate; sodium tris(acetoxy)borohydride; orthoformic acid triethyl ester;
In
methanol; ethanol; dichloromethane; water;
DOI:10.1016/j.bmcl.2013.01.072
