6c-(4-Methylthiophenyl)-1,6b-diphenyl-2-oxo-1,2,4,5,6,6a,6b,6c-octahydrocyclopropindolizin

Base Information

• Chemical Name: 6c-(4-Methylthiophenyl)-1,6b-diphenyl-2-oxo-1,2,4,5,6,6a,6b,6c-octahydrocyclopropindolizin
• CAS No.: 108201-26-9
• Molecular Formula: C₂₇H₂₅NOS
• Molecular Weight: 411.568

Synonyms:6c-(4-Methylthiophenyl)-1,6b-diphenyl-2-oxo-1,2,4,5,6,6a,6b,6c-octahydrocyclopropindolizin

Chemical Property of 6c-(4-Methylthiophenyl)-1,6b-diphenyl-2-oxo-1,2,4,5,6,6a,6b,6c-octahydrocyclopropindolizin

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Technology Process of 6c-(4-Methylthiophenyl)-1,6b-diphenyl-2-oxo-1,2,4,5,6,6a,6b,6c-octahydrocyclopropindolizin

There total 2 articles about 6c-(4-Methylthiophenyl)-1,6b-diphenyl-2-oxo-1,2,4,5,6,6a,6b,6c-octahydrocyclopropindolizin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

6c-(4-Methylthiophenyl)-1,6b-diphenyl-2-thioxo-1,2,4,5,6,6a,6b,6c-octahydrocyclopropindolizin (108201-34-9) → 6c-(4-Methylthiophenyl)-1,6b-diphenyl-2-oxo-1,2,4,5,6,6a,6b,6c-octahydrocyclopropindolizin (108201-26-9)

Guidance literature:

With mesitylenecarbonitrile oxide; In acetonitrile; Heating;

DOI:10.1055/s-1986-31820

Reference yield: 22.0%

6-(4-methylsulfanyl-phenyl)-2,3,4,5-tetrahydro-pyridine (91642-78-3) + diphenylcyclopropenone (886-38-4) → 6c-(4-Methylthiophenyl)-1,6b-diphenyl-2-oxo-1,2,4,5,6,6a,6b,6c-octahydrocyclopropindolizin (108201-26-9) + 5-(4-Methylthiophenyl)-2,3-diphenyl-1-azabicyclo<4.3.0>non-2-en-4-on (108201-19-0)

Guidance literature:

In butan-1-ol; 1.) reflux, 3 h, 2.) 20 deg C, 15 h;

DOI:10.1055/s-1986-31820

Reference yield: 76.0%

6c-(4-Methylthiophenyl)-1,6b-diphenyl-2-oxo-1,2,4,5,6,6a,6b,6c-octahydrocyclopropindolizin (108201-26-9) → 6c-(4-Methylthiophenyl)-1,6b-diphenyl-2-thioxo-1,2,4,5,6,6a,6b,6c-octahydrocyclopropindolizin (108201-34-9)

Guidance literature:

With Lawessons reagent; In N,N,N,N,N,N-hexamethylphosphoric triamide; at 100 ℃;

DOI:10.1055/s-1986-31820

upstream raw materials:

6c-(4-Methylthiophenyl)-1,6b-diphenyl-2-thioxo-1,2,4,5,6,6a,6b,6c-octahydrocyclopropindolizin

6-(4-methylsulfanyl-phenyl)-2,3,4,5-tetrahydro-pyridine

diphenylcyclopropenone

Downstream raw materials:

6c-(4-Methylthiophenyl)-1,6b-diphenyl-2-thioxo-1,2,4,5,6,6a,6b,6c-octahydrocyclopropindolizin

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