C₄₂H₃₈N₂O₉

Base Information

Chemical Name:C₄₂H₃₈N₂O₉
CAS No.:1422958-91-5
Molecular Formula:C₄₂H₃₈N₂O₉
Molecular Weight:714.772
Hs Code.:

C<sub>42</sub>H<sub>38</sub>N<sub>2</sub>O<sub>9</sub>

Synonyms:C₄₂H₃₈N₂O₉

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Chemical Property of C₄₂H₃₈N₂O₉

Chemical Property:

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Technology Process of C₄₂H₃₈N₂O₉

There total 18 articles about C₄₂H₃₈N₂O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 1422958-90-4
1-(5-(N-(phenoxyacetyl)amino)phthalimid-3-yl)-1,2-dideoxy-β-D-ribofuranose

: DMT-Cl

: 1422958-91-5
C₄₂H₃₈N₂O₉

Guidance literature:: With pyridine; at 20 ℃; for 42h;
DOI:10.1021/jo302768f

Reference yield:

: 1975-52-6
5-nitro-o-toluic acid

: 1422958-91-5
C₄₂H₃₈N₂O₉

Guidance literature:: Multi-step reaction with 10 steps

1: N-Bromosuccinimide; sulfuric acid / 2.5 h / 60 °C

2: sodium hydroxide; potassium permanganate / water / 60 - 100 °C

3: urea / o-xylene / 4 h / 160 °C

4: tris(pentafluorophenyl)phosphine; triethylamine; palladium diacetate / acetonitrile / 82 °C / Inert atmosphere

5: sodium tris(acetoxy)borohydride / acetonitrile / 1 h / 0 °C / Inert atmosphere

6: pyridine; 1H-imidazole / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

7: sodium hydrogen sulfide / ethanol; water / 1 h / 78 °C

8: pyridine / 20 °C / Inert atmosphere

9: triethylamine tris(hydrogen fluoride) / tetrahydrofuran / 20 °C / Inert atmosphere

10: pyridine / 42 h / 20 °C

With pyridine; 1H-imidazole; sodium hydrogen sulfide; potassium permanganate; N-Bromosuccinimide; sulfuric acid; palladium diacetate; sodium tris(acetoxy)borohydride; triethylamine tris(hydrogen fluoride); triethylamine; urea; tris(pentafluorophenyl)phosphine; sodium hydroxide; In tetrahydrofuran; ethanol; o-xylene; water; N,N-dimethyl-formamide; acetonitrile; 4: |Heck Reaction;
DOI:10.1021/jo302768f

Reference yield:

: 1422958-85-7
3-iodo-5-nitrophthalimide

: 1422958-91-5
C₄₂H₃₈N₂O₉

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydrogen sulfide / ethanol; water / 1 h / 78 °C

2: pyridine; 1H-imidazole / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

3: tris(pentafluorophenyl)phosphine; triethylamine; palladium diacetate / acetonitrile / 82 °C / Inert atmosphere

4: sodium tris(acetoxy)borohydride; acetic acid / acetonitrile / 1 h / 0 °C / Inert atmosphere

5: pyridine / 42 h / 20 °C

With pyridine; 1H-imidazole; sodium hydrogen sulfide; palladium diacetate; sodium tris(acetoxy)borohydride; acetic acid; triethylamine; tris(pentafluorophenyl)phosphine; In tetrahydrofuran; ethanol; water; acetonitrile; 3: |Heck Reaction;
DOI:10.1021/jo302768f