2,5-anhydro-4,6-di-O-benzoyl-3-deoxy-N-(2-pyridylmethyl)-D-ribo-hexonamide

Base Information

Chemical Name:2,5-anhydro-4,6-di-O-benzoyl-3-deoxy-N-(2-pyridylmethyl)-D-ribo-hexonamide
CAS No.:98748-22-2
Molecular Formula:C₂₆H₂₄N₂O₆
Molecular Weight:460.486
Hs Code.:

Synonyms:2,5-anhydro-4,6-di-O-benzoyl-3-deoxy-N-(2-pyridylmethyl)-D-ribo-hexonamide

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Chemical Property of 2,5-anhydro-4,6-di-O-benzoyl-3-deoxy-N-(2-pyridylmethyl)-D-ribo-hexonamide

Chemical Property:

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Technology Process of 2,5-anhydro-4,6-di-O-benzoyl-3-deoxy-N-(2-pyridylmethyl)-D-ribo-hexonamide

There total 6 articles about 2,5-anhydro-4,6-di-O-benzoyl-3-deoxy-N-(2-pyridylmethyl)-D-ribo-hexonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 84562-04-9
(4S,trans)-4-benzoyloxy-5-benzoyloxymethyl-4,5-dihydrofuran-N-(2-pyridylmethyl)furan-2-carboxamide

: 98748-22-2,98748-25-5
C₂₆H₂₄N₂O₆

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; under 760 Torr;
DOI:10.1016/0008-6215(82)85041-6

Reference yield:

: 84562-04-9
(4S,trans)-4-benzoyloxy-5-benzoyloxymethyl-4,5-dihydrofuran-N-(2-pyridylmethyl)furan-2-carboxamide

: 98748-22-2
2,5-anhydro-4,6-di-O-benzoyl-3-deoxy-N-(2-pyridylmethyl)-D-ribo-hexonamide

: 98748-25-5
2,5-anhydro-4,6-di-O-benzoyl-3-deoxy-N-(2-pyridylmethyl)-D-arabino-hexonamide

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; for 96h; under 760 Torr; Yield given. Yields of byproduct given;
DOI:10.1039/P19850000621

Reference yield:

: 3731-51-9
2-(Aminomethyl)pyridine

: 98748-22-2,98748-25-5
C₂₆H₂₄N₂O₆

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / 2-chloro-N-methylpyridinium iodide, Et₃N / acetonitrile / Ambient temperature

2: H₂ / Pd-C / ethyl acetate / 760 Torr

With 2-chloro-1-methyl-pyridinium iodide; hydrogen; triethylamine; palladium on activated charcoal; In ethyl acetate; acetonitrile;
DOI:10.1016/0008-6215(82)85041-6