(S)-Pyrrolidine-1,2-dicarboxylic acid 2-{[(S)-1-(benzyl-methyl-carbamoyl)-2-naphthalen-2-yl-ethyl]-amide} 1-{[2-(tert-butyl-dimethyl-silanyloxy)-phenyl]-amide}

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Chemical Name:(S)-Pyrrolidine-1,2-dicarboxylic acid 2-{[(S)-1-(benzyl-methyl-carbamoyl)-2-naphthalen-2-yl-ethyl]-amide} 1-{[2-(tert-butyl-dimethyl-silanyloxy)-phenyl]-amide}
CAS No.:212701-49-0
Molecular Formula:C₃₉H₄₈N₄O₄Si
Molecular Weight:664.92
Hs Code.:

(S)-Pyrrolidine-1,2-dicarboxylic acid 2-{[(S)-1-(benzyl-methyl-carbamoyl)-2-naphthalen-2-yl-ethyl]-amide} 1-{[2-(tert-butyl-dimethyl-silanyloxy)-phenyl]-amide}

Synonyms:(S)-Pyrrolidine-1,2-dicarboxylic acid 2-{[(S)-1-(benzyl-methyl-carbamoyl)-2-naphthalen-2-yl-ethyl]-amide} 1-{[2-(tert-butyl-dimethyl-silanyloxy)-phenyl]-amide}

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Chemical Property of (S)-Pyrrolidine-1,2-dicarboxylic acid 2-{[(S)-1-(benzyl-methyl-carbamoyl)-2-naphthalen-2-yl-ethyl]-amide} 1-{[2-(tert-butyl-dimethyl-silanyloxy)-phenyl]-amide}

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Technology Process of (S)-Pyrrolidine-1,2-dicarboxylic acid 2-{[(S)-1-(benzyl-methyl-carbamoyl)-2-naphthalen-2-yl-ethyl]-amide} 1-{[2-(tert-butyl-dimethyl-silanyloxy)-phenyl]-amide}

There total 2 articles about (S)-Pyrrolidine-1,2-dicarboxylic acid 2-{[(S)-1-(benzyl-methyl-carbamoyl)-2-naphthalen-2-yl-ethyl]-amide} 1-{[2-(tert-butyl-dimethyl-silanyloxy)-phenyl]-amide} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 165405-44-7
2-(tert-butyldimethylsilanyloxy)phenyl isocyanate

: (S)-Pyrrolidine-2-carboxylic acid [(S)-1-(benzyl-methyl-carbamoyl)-2-naphthalen-2-yl-ethyl]-amide

: 212701-49-0
(S)-Pyrrolidine-1,2-dicarboxylic acid 2-{[(S)-1-(benzyl-methyl-carbamoyl)-2-naphthalen-2-yl-ethyl]-amide} 1-{[2-(tert-butyl-dimethyl-silanyloxy)-phenyl]-amide}

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; Ambient temperature;
DOI:10.1021/jm970499g

Reference yield:

: 69589-21-5
O-tert-butyldimethylsilyl-2-aminophenol

: 212701-49-0
(S)-Pyrrolidine-1,2-dicarboxylic acid 2-{[(S)-1-(benzyl-methyl-carbamoyl)-2-naphthalen-2-yl-ethyl]-amide} 1-{[2-(tert-butyl-dimethyl-silanyloxy)-phenyl]-amide}

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 1 h / 60 °C

2: 73 percent / Et₃N / dimethylformamide / Ambient temperature

With triethylamine; In N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm970499g